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Benzyl Benzoate, Phenylmethyl Benzoate, Benzyl Phenyl Formate, 120-51-4

Benzyl Benzoate, Phenylmethyl Benzoate, Benzyl Phenyl Formate, 120-51-4

BENZYL BENZOATE

PRODUCT IDENTIFIER INFORMATION

Parameter Information
Product Name Benzyl Benzoate
Chemical Name (IUPAC) Phenylmethyl Benzoate
CAS Number 120-51-4
EC Number (EINECS) 204-402-9
FEMA Number 2138
JECFA Number 24
Molecular Formula C14H12O2
Molecular Weight 212.24 g/mol

SECTION 1: CHEMICAL IDENTITY AND DESCRIPTION

Parameter Information
Chemical Name (IUPAC) Phenylmethyl Benzoate
Systematic Name Benzoic Acid Phenylmethyl Ester
Synonyms Benzyl Benzoate, Benzyl Phenylformate, Benzyl Alcohol Benzoic Ester, Benzoic Acid Benzyl Ester, Benzyl Benzene Carboxylate, Phenylmethyl Benzoate
Trade Names Ascabin, Benylate, Ascabiol, Scabagen, Vanzoate, Venzonate
CAS Number 120-51-4
EC Number (EINECS) 204-402-9
FEMA Number 2138
JECFA Number 24
Molecular Formula C14H12O2
Molecular Weight 212.24 g/mol
Chemical Class Organic ester (benzoic acid benzyl ester)
Physical State (20°C) Liquid (colorless oily liquid; pure form is flaky crystalline solid below 17°C)
Odor Weak balsamic, almond-like aroma
Appearance Clear colorless transparent liquid; slightly viscous

SECTION 2: PHYSICAL AND CHEMICAL PROPERTIES

Property Value Test Method
Appearance Clear colorless transparent oily liquid; slightly viscous Visual
Color Clear colorless Visual
Odor Weak balsamic, almond-like aroma Olfactometric
Molecular Weight 212.24 g/mol Calculated
Melting/Freezing Point 17 – 21°C (solidifies below this range) DSC
Boiling Point 323 – 324°C ASTM D86
Flash Point 148°C (298°F) ASTM D93
Autoignition Temperature 480°C (896°F) ASTM E659
Density (20°C) 1.118 g/mL ASTM D4052
Refractive Index (nD20) 1.568 – 1.570 Refraktometri
Vapor Pressure (125°C) 1 mmHg ASTM D2879
Solubility in Water Practically insoluble Genel Metot
Solubility in Ethanol Miscible Genel Metot
Solubility in Chloroform Miscible Genel Metot
Solubility in Ether Miscible Genel Metot
Solubility in Oils Miscible Genel Metot
Solubility in Glycerol Insoluble Genel Metot
Log P (Octanol/Water) ~4 (at 20°C) Hesaplanmış
Stability Stable under normal conditions; light-sensitive; combustible  

SECTION 3: CHEMICAL PROPERTIES AND REACTIVITY

Parameter Information
Chemical Character Organic ester; fixative and solvent
Stability Stable under normal conditions; light-sensitive
Decomposition Products (Heating) CO, CO2, irritating fumes
Incompatible Materials Strong oxidizing agents, strong acids, strong bases
Reaction with Oxidizing Agents Intense reaction with strong oxidizers
Hydrolysis Slowly hydrolyzes in presence of strong acids or bases to benzoic acid and benzyl alcohol
Light Sensitivity Sensitive to light; store in dark conditions
Volatility Can volatilize with water vapor
Hazardous Polymerization Does not occur

SECTION 4: PRODUCTION METHODS

Method Description Chemical Reaction
Transesterification Ethyl benzoate reacted with benzyl alcohol in presence of sodium carbonate catalyst; ethanol removed by distillation; product purified by vacuum distillation C6H5COOCH2CH3 + C6H5CH2OH → C6H5COOCH2C6H5 + CH3CH2OH
Benzaldehyde Condensation Sodium metal dissolved in benzyl alcohol; benzaldehyde slowly added; reaction in water bath for 1-2 hours; oil layer separated, washed, and fractionated 2C6H5CHO → C6H5COOCH2C6H5
Sodium Benzoate Route Sodium benzoate reacted with benzoyl chloride in presence of triethylamine C6H5COONa + C6H5COCl → C6H5COOCH2C6H5 + NaCl
Natural Occurrence Found naturally in Peruvian balsam, tuberose, carnation, and tolu balsam -

SECTION 5: BENZOATE ESTERS COMPARISON

Property Benzyl Benzoate Methyl Benzoate Ethyl Benzoate Benzyl Acetate Benzyl Salicylate
CAS Number 120-51-4 93-58-3 93-89-0 140-11-4 118-58-1
Molecular Formula C14H12O2 C8H8O2 C9H10O2 C9H10O2 C14H12O3
Molecular Weight 212.24 136.15 150.17 150.17 228.24
Boiling Point 323-324°C 199°C 212°C 213°C 320°C
Odor Balsamic, almond Fruity, floral Fruity, grape Floral, jasmine Mild floral, balsamic
Primary Use Fixative, solvent, pharmaceutical Flavor, solvent Flavor, fragrance Fragrance, flavor Fragrance fixative, sunscreen
Water Solubility Insoluble Slightly soluble Slightly soluble Slightly soluble Insoluble

SECTION 6: FUNCTIONAL PROPERTIES AND MECHANISM OF ACTION

Property Description
Fragrance Fixative Reduces evaporation rate of volatile fragrance components; extends longevity of perfume compositions
Solvent for Solid Aromatics Excellent solvent for solid fragrances; dissolves 0.45 kg musk ambrette, 0.205 kg musk ketone, or 0.28 kg musk xylene per kg
Plasticizer Used as plasticizer in cellulose acetate and other polymer systems
Scabicide (Pharmaceutical) Active ingredient in scabies treatment; penetrates mite exoskeleton causing paralysis and death
Insect Repellent Effective against certain insects; used in textile and agricultural applications
Dye Carrier (Textile) Used as dye guide, leveling agent, and repair agent in textile auxiliaries, especially for polyester
Flavoring Agent Used in food flavor formulations (strawberry, pineapple, cherry, etc.)
High-Boiling Solvent High boiling point (323°C) makes it suitable as high-temperature solvent

SECTION 7: PRIMARY APPLICATION AREAS

Sector Application Typical Usage Rate
Fragrance Industry Fixative in floral fragrances (jasmine, lily of the valley, ylang-ylang, gardenia, lilac, tuberose) 1 – 30% of composition
Fragrance Industry Solvent for solid aromatics (musk ambrette, musk ketone, musk xylene) As required
Flavor Industry Food flavoring: soft drinks (4.5 mg/kg), candy (39 mg/kg), baked goods (33 mg/kg), chewing gum (280 mg/kg), cold drinks (12 mg/kg) Per FEMA limits
Pharmaceutical Scabicide – scabies treatment lotion/cream 10 – 25% topical
Pharmaceutical Preparation of pertussis (whooping cough) medicine, asthma medicine Formulation dependent
Pharmaceutical Antispasmodic agent Formulation dependent
Textile Dye carrier, leveling agent, repair agent (especially polyester) Variable
Industrial Plasticizer for cellulose acetate Variable
Agricultural Pesticide intermediate Variable
Cosmetic Fragrance component in creams, lotions, and personal care products 0.1 – 5%

SECTION 8: QUALITY SPECIFICATIONS (TECHNICAL/FRAGRANCE GRADE)

Parameter Specification Test Method
Appearance Clear colorless transparent liquid Visual
Odor Weak balsamic, almond-like aroma Olfactometric
Purity (Ester Content) ≥ 99.0% GC-FID
Acidity (as Benzoic Acid) ≤ 0.1% Titrimetric
Refractive Index (nD20) 1.568 – 1.570 Refraktometri
Density (20°C) 1.116 – 1.120 g/mL ASTM D4052
Freezing Point ≥ 17°C DSC
Flash Point ≥ 148°C ASTM D93
Water Content ≤ 0.1% Karl Fischer Titrasyonu
Heavy Metals (as Pb) ≤ 10 ppm ICP-MS
Lead (Pb) ≤ 2 ppm ICP-MS
Arsenic (As) ≤ 3 ppm ICP-MS
Color (APHA) ≤ 50 ASTM D1209

SECTION 9: TOXICOLOGICAL PROFILE

Parameter Value
Acute Oral Toxicity (LD50, Rat) ~1,700 mg/kg
Acute Oral Toxicity (LD50, Mouse) ~1,400 mg/kg
Acute Oral Toxicity (LD50, Rabbit) ~1,800 mg/kg
Acute Oral Toxicity (LD50, Guinea Pig) ~1,000 mg/kg
Acute Dermal Toxicity (LD50, Rabbit) > 2,000 mg/kg
Skin Irritation Mild irritant
Eye Irritation Irritant (avoid eye contact)
Respiratory Irritation May cause respiratory irritation
Carcinogenicity Not classified (IARC, NTP)
Mutagenicity Negative in standard tests
ADI (Acceptable Daily Intake) 0 – 5 mg/kg (FAO/WHO, 1994)
Environmental Toxicity Toxic to aquatic organisms (R51/53); may cause long-term adverse effects

SECTION 10: GHS CLASSIFICATION AND LABELING

GHS Classification (compliant with 1272/2008/EC):

Hazard Class Category H-Statement
Acute Toxicity (Oral) Category 4 H302
Chronic Aquatic Toxicity Category 2 H411

Signal Word: WARNING

Hazard Pictograms: GHS07 (Exclamation Mark), GHS09 (Environmental Toxicity)

Hazard Statements (H-Codes):

Code Statement
H302 Harmful if swallowed
H411 Toxic to aquatic life with long lasting effects

Precautionary Statements (P-Codes):

Code Statement
P264 Wash hands thoroughly after handling
P270 Do not eat, drink or smoke when using this product
P273 Avoid release to the environment
P280 Wear protective gloves/eye protection
P301+P312 IF SWALLOWED: Call a POISON CENTER/doctor if you feel unwell
P391 Collect spillage
P501 Dispose of contents/container to approved waste disposal facility

SECTION 11: FIRST AID MEASURES

Exposure Route Action to Take
Inhalation Move to fresh air. Seek medical attention if respiratory irritation persists.
Skin Contact Wash with plenty of water and soap. Remove contaminated clothing. Seek medical attention if irritation persists.
Eye Contact Rinse immediately with plenty of water for at least 15 minutes. Remove contact lenses if present. Seek medical attention.
Ingestion Rinse mouth with water. Do NOT induce vomiting. Seek immediate medical attention and show container or label.

SECTION 12: FIREFIGHTING MEASURES

Parameter Information
Fire Hazard Combustible liquid
Flash Point 148°C (298°F)
Autoignition Temperature 480°C (896°F)
Hazards During Fire Releases CO, CO2, irritating fumes
Suitable Extinguishing Media Dry powder, CO2, water mist (fog), alcohol-resistant foam
Special Protective Equipment Self-contained breathing apparatus (SCBA), full protective clothing

SECTION 13: STORAGE AND SHELF LIFE

Parameter Information
Storage Conditions Cool (2-8°C recommended), dark, dry, well-ventilated area
Container Requirements Tightly closed, light-resistant containers
Keep Away From Light (light-sensitive), strong oxidizing agents, strong acids, strong bases
Freezing Note Solidifies below 17°C; if frozen, place container in drying room (35-70°C) or warm water bath (40-90°C) to melt before use
Shelf Life 24 months (unopened original packaging under appropriate storage conditions)
Stability Note Light-sensitive; combustible; store in dark, cool environment

SECTION 14: PACKAGING OPTIONS

Packaging Type Quantity Material
HDPE drum 25 kg HDPE (light-protected)
HDPE drum 50 kg HDPE (light-protected)
HDPE drum 200 kg HDPE (light-protected)
IBC Container 1000 kg HDPE
Glass bottle (laboratory) 1-5 kg Amber glass

SECTION 15: TRANSPORTATION INFORMATION

Parameter Information
UN Number UN 3082 (Environmentally Hazardous Substance, Liquid, n.o.s.)
Hazard Class 9 (Environmentally Hazardous Substances)
Packing Group III
ADR/RID UN 3082, Environmentally Hazardous Substance, 9, PG III
IMDG Code UN 3082, Environmentally Hazardous Substance, 9, PG III
IATA (Air) UN 3082, Environmentally Hazardous Substance, 9, PG III
Marine Pollutant Yes
Transport Temperature Ambient; protect from light and freezing

SECTION 16: REGULATORY STATUS

Region / Authority Status
USA (FDA) Approved as flavoring agent (21 CFR 172.515); moderate limit
FEMA 2138 – approved for food flavor use
JECFA (FAO/WHO) Evaluated; ADI 0-5 mg/kg
European Union Approved as flavoring substance; cosmetic ingredient
Turkey Approved under Turkish Food Codex Flavoring Regulation
Pharmaceutical USP/EP monographs available for pharmaceutical grade

SECTION 17: OTHER NAMES AND SYNONYMS

Type Name
Chemical Names Benzyl Benzoate, Phenylmethyl Benzoate, Benzoic Acid Benzyl Ester, Benzoic Acid Phenylmethyl Ester
Other Chemical Names Benzyl Phenylformate, Benzyl Alcohol Benzoic Ester, Benzyl Benzene Carboxylate
Trade Names Ascabin, Benylate, Ascabiol, Scabagen, Vanzoate, Venzonate
CAS Number 120-51-4
EC Number 204-402-9
FEMA Number 2138

SECTION 18: SUMMARY TABLE

Parameter Value
Product Benzyl Benzoate
CAS Number 120-51-4
Molecular Formula C14H12O2
Molecular Weight 212.24 g/mol
Appearance Clear colorless transparent oily liquid
Boiling Point 323 – 324°C
Freezing Point 17 – 21°C
Density (20°C) 1.118 g/mL
Odor Weak balsamic, almond-like
Primary Function Fragrance fixative, solvent for solid aromatics, scabicide, flavoring agent
Shelf Life 24 months
GHS Signal Word Warning
UN Number UN 3082 (Environmentally Hazardous, 9, PG III)

SECTION 19: CRITICAL WARNINGS AND BEST PRACTICES

CRITICAL WARNINGS:

  1. Freezing Point: Solidifies below 17°C; must be completely melted before use. Place container in warm water bath (40-90°C) or drying room (35-70°C) to melt.

  2. Light Sensitivity: Sensitive to light; store in dark, light-resistant containers.

  3. Aquatic Toxicity: Toxic to aquatic organisms with long lasting effects; do not release to the environment.

  4. Harmful if Swallowed: May cause gastrointestinal irritation; do not induce vomiting.

  5. Combustible: Keep away from heat, sparks, and open flames.

BEST PRACTICE RECOMMENDATIONS:

  1. Melting Procedure: In winter, place solidified benzyl benzoate container in warm water bath (40-90°C) or drying room (35-70°C) until completely liquefied before use.

  2. Solid Fragrance Solvent: Use as solvent for solid fragrances: 1 kg benzyl benzoate dissolves 0.45 kg musk ambrette, 0.205 kg musk ketone, or 0.28 kg musk xylene.

  3. Fragrance Fixative: Use at 1-30% in fragrance compositions to extend longevity of volatile notes.

  4. Storage: Store at 2-8°C in dark, well-ventilated area; protect from light.

  5. Handling: Use protective gloves and goggles; avoid eye contact (S25).

LEGAL DISCLAIMER:

The information provided in this document is presented in good faith based on our current knowledge and experience; however, since all usage conditions are beyond our control, it does not constitute a binding specification or warranty. This Technical Data Sheet is for informational purposes only. Users are obligated to test the suitability for their own applications. For complete safety, storage, handling, transportation, disposal, and regulatory compliance information, refer to the official Safety Data Sheet (SDS/MSDS) provided by the manufacturer/supplier.

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