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Nickel Sulfamate, Nickel Sulfamate Tetrahydrate, Nickel Sulfamate Anhydrous, Nickel Amidosulfonate, 124594-15-6, 13770-89-3

Nickel Sulfamate, Nickel Sulfamate Tetrahydrate, Nickel Sulfamate Anhydrous, Nickel Amidosulfonate, 124594-15-6, 13770-89-3

NICKEL SULFAMATE

1. PRODUCT IDENTIFICATION AND CHEMICAL IDENTITY

Parameter Description
Chemical Name Nickel(II) sulfamate tetrahydrate
Other Names Nickel sulfamate tetrahydrate, Nickel(II) amidosulfonate tetrahydrate
CAS Number 124594-15-6 (hydrate) / 13770-89-3 (anhydrous)
EC Number (EINECS) 237-396-1
Chemical Formula Ni(SO₃NH₂)₂·4H₂O
Molecular Weight 322.92 g/mol (tetrahydrate) / 250.85 g/mol (anhydrous)
Chemical Class Transition metal sulfamate salt / Inorganic salt
Appearance Clear green liquid or green crystalline powder
Odor Slight odorless or ammonia-like
Density ~1.52-1.58 g/cm³ (solution)
pH (Aqueous Solution) ~4.0-5.0

CHEMICAL STRUCTURE AND DESCRIPTION:

Nickel Sulfamate (Ni(SO₃NH₂)₂·4H₂O) is the sulfamate salt of nickel in the +2 oxidation state. It consists of a nickel ion (Ni²⁺) and two sulfamate ions (SO₃NH₂⁻). It is hygroscopic and highly soluble in water. Commercially, it is typically supplied as a 50-60% aqueous solution. It is used in the electroplating industry for high-quality nickel plating baths, in electronic and precision engineering applications. Nickel sulfamate baths produce low-stress, soft, and ductile nickel deposits compared to nickel chloride baths.

Structural Features:

  • Nickel ion in +2 oxidation state

  • Two sulfamate ligands (SO₃NH₂⁻)

  • Tetrahydrate form (4 water molecules)

  • Highly soluble in water

  • Hygroscopic

  • Supplied as aqueous solution

2. PHYSICAL AND CHEMICAL PROPERTIES

Property Value
Chemical Formula Ni(SO₃NH₂)₂·4H₂O
Molecular Weight 322.92 g/mol (tetrahydrate)
Appearance Clear green liquid or green crystalline powder
Odor Slight odorless / ammonia-like
Density ~1.52-1.58 g/cm³ (solution)
pH (50% Solution) ~4.0-5.0
Solubility in Water High
Solubility in Organic Solvents Limited
Hygroscopicity Hygroscopic

3. SOLUBILITY PROFILE

Solvent Solubility
Water High
Organic Solvents Limited

4. APPLICATIONS AND INDUSTRIAL USES

Sector Application
Electroplating High-quality nickel plating baths
Electronics Precision engineering coatings
Metal Surface Treatment Metal surface cleaning and protection
Battery Technology Active material precursor for nickel-metal hydride batteries
Catalysts Chemical synthesis catalysts

Sulfamate Bath Advantages:

  • Low internal stress deposits

  • Soft and ductile nickel layers

  • High plating speed

  • Excellent throwing power

  • Pure nickel deposits

  • Lower internal stress compared to nickel chloride baths

5. SPECIFICATIONS (TYPICAL)

Parameter Specification
Purity ≥ 99.0%
Appearance Clear green liquid
Nickel Content (Ni) ~17-19%
pH (50% Solution) 4.0-5.0
Water Solubility Complete
Density 1.52-1.58 g/cm³
Metals (Fe, Cu, Zn) ≤ 0.005%
Chloride (Cl) ≤ 0.01%
Sulfate (SO₄) ≤ 0.005%

6. HANDLING AND STORAGE

Parameter Information
Storage Conditions Cool, dry, well-ventilated area
Storage Temperature 15-25°C
Keep Away From Strong oxidizers, acids, moisture
Shelf Life 12-24 months (under proper storage)
Packaging Tightly closed plastic containers
UN Number Not classified as dangerous for transport

Handling Notes:

  • Nickel compounds may cause allergic reactions

  • Use only in well-ventilated areas

  • Avoid skin and eye contact

  • Hygroscopic; protect from moisture

7. SAFETY AND TOXICOLOGY

Parameter Value
GHS Classification GHS07, GHS08, GHS09
Signal Word Danger
Hazard Statements H302 (Harmful if swallowed), H315 (Skin irritation), H317 (May cause allergic skin reaction), H319 (Serious eye irritation), H332 (Harmful if inhaled), H335 (Respiratory tract irritation), H341 (Suspected of causing genetic defects), H351 (Suspected of causing cancer), H360 (May damage fertility or unborn child), H372 (Causes damage to organs), H410 (Very toxic to aquatic life)
Precautionary Statements P201, P260, P280, P301+P310, P304+P340, P308+P313
Toxicity Harmful if swallowed or inhaled
Exposure Routes Inhalation, ingestion, skin contact
Symptoms Skin sensitization, respiratory tract irritation, nausea
Target Organs Respiratory system, skin, reproductive system
Carcinogenicity Category 1B (suspected carcinogen)
Reproductive Toxicity Category 1
Ecotoxicity Very toxic to aquatic life

Personal Protective Equipment:

  • Chemical-resistant gloves

  • Safety goggles

  • Protective clothing

  • Respiratory protection (dust/vapor mask)

  • Adequate ventilation must be provided

  • Regular health check-ups (nickel exposure)

8. ENVIRONMENTAL INFORMATION

Parameter Information
Ecotoxicity Very toxic to aquatic organisms
Bioaccumulation Nickel compounds accumulate in the environment
Environmental Impact Must be prevented from entering water and soil sources
Waste Management Nickel-containing waste must be processed at specialized disposal facilities

9. FIRST AID MEASURES

Exposure Route Action
Inhalation Move to fresh air. If breathing difficulty occurs, administer oxygen. Seek medical attention.
Skin Contact Remove contaminated clothing. Wash with plenty of water and soap. Seek medical attention.
Eye Contact Rinse with plenty of water for at least 15 minutes. Seek medical attention.
Ingestion Do NOT induce vomiting. Rinse mouth with water. Drink plenty of water. Seek medical attention.

10. TRANSPORT INFORMATION

Parameter Information
UN Number Not classified as dangerous for transport
Hazard Class Not classified
Packing Group Not applicable
Proper Shipping Name Nickel Sulfamate
Marine Pollutant Yes
ADR/RID Label None

11. REGULATORY INFORMATION

Region Status
EU REACH registered
Turkey (KKDİK) Mandatory compliance; registration required
USA (TSCA) Listed
EINECS 237-396-1
Customs Tariff Code 2833.30.00.00

12. SUMMARY AND CRITICAL WARNINGS

SUMMARY:

Nickel Sulfamate (Ni(SO₃NH₂)₂·4H₂O, CAS 13770-89-3) is a clear green liquid or green crystalline solid. It is highly soluble in water and hygroscopic. Commercially, it is typically supplied as a 50-60% aqueous solution.

Its most important applications include use in electroplating (high-quality nickel plating baths), in electronic and precision engineering applications, and in metal surface treatment.

Nickel Sulfamate baths produce low-stress, soft, and ductile nickel deposits compared to nickel chloride baths. They offer high plating speed and excellent throwing power.

Nickel compounds may cause allergic reactions and long-term cancer risk. Harmful if swallowed or inhaled. Causes skin irritation, allergic skin reactions, and respiratory tract irritation. Very toxic to aquatic life. Storage should be in cool, dry, well-ventilated areas, in tightly closed containers, away from strong oxidizers and acids.

Key Properties:

Property Value
Formula Ni(SO₃NH₂)₂·4H₂O
CAS No 13770-89-3
Molecular Weight 322.92 g/mol
Appearance Clear green liquid / green crystal
Water Solubility High
Density ~1.52-1.58 g/cm³
pH 4.0-5.0

CRITICAL WARNINGS:

  1. Carcinogenicity: Nickel compounds are classified as Category 1B carcinogens (H351).

  2. Allergic Reactions: Skin contact may cause allergic reactions (H317). Inhalation may cause allergy or asthma symptoms (H334).

  3. Reproductive Toxicity: May damage fertility or unborn child (H360).

  4. Organ Damage: Prolonged exposure causes organ damage (H372).

  5. Environmental: Very toxic to aquatic life with long-lasting effects (H410). Must be prevented from entering water and soil sources.

  6. Hygroscopic: Protect from moisture. Store in tightly closed containers.

  7. Waste Management: Nickel-containing waste must be processed at specialized disposal facilities.

Important Disclaimer: This Technical Data Sheet (TDS) is for informational purposes only. The information provided is based on available data and is believed to be accurate. However, the user is solely responsible for determining the suitability of the product for their specific applications and for complying with all applicable regulations and safety requirements. For complete safety, handling, storage, and regulatory compliance information, always refer to the official Safety Data Sheet (SDS/MSDS) provided by the manufacturer/supplier. All local, national, and international regulations must be followed when working with Nickel Sulfamate.

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