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Metakaolin, Meta Kaolin, Calcined Kaolin, 15123-81-6

Metakaolin, Meta Kaolin, Calcined Kaolin, 15123-81-6

METAKAOLIN

1. PRODUCT IDENTIFICATION

Parameter Information
Product Name Metakaolin
CAS Number 15123-81-6
Chemical Formula Al₂O₇Si₂ (Metakaolinite)
Molecular Weight ~222 g/mol
Definition High-pozzolanic activity, fine particulate mineral admixture obtained by controlled calcination (600-900°C) of kaolinite mineral
Appearance Grey – light brown powder
Odor No characteristic mineral odor
Physical State (20°C) Solid (powder)

2. CHEMICAL STRUCTURE AND MOLECULAR PROPERTIES

2.1. Chemical Structure

Metakaolin is formed by the thermal dehydroxylation of kaolinite (Al₂Si₂O₅(OH)₄). During calcination, the layered structure of kaolinite breaks down as hydroxyl groups (OH) are removed, resulting in an amorphous, highly reactive structure.

Reaction:

Kaolinite (Al₂Si₂O₅(OH)₄)  →  Metakaolin (Al₂O₇Si₂)  +  2H₂O↑
(600-900°C)                      (Amorphous)

2.2. Crystal Structure

Feature Description
Crystal Structure Initially layered structure of kaolinite becomes disordered (amorphous) after calcination
Specific Surface Area 10 – 20 m²/g (measured by Blaine method)
Pozzolanic Activity High; reacts with Ca(OH)₂ due to amorphous silica and alumina content
XRD Characteristics Characteristic peaks of kaolinite disappear after calcination; amorphous halo is observed

3. CHEMICAL COMPOSITION (average values)

Component % (approx.) Description
SiO₂ 50 – 63 Main component; primary source of pozzolanic activity
Al₂O₃ 19 – 35 High alumina content; enhances reactivity
Na₂O 0.1 – 0.5 Alkali content; may vary by source
CaO 0.3 – 5 Impurity; may indicate limestone residue in some ores
Fe₂O₃ 0.1 – 1 Color-imparting impurity; undesirable in light-colored products
K₂O 1 – 2 Alkali content; requires attention for ASR reactions
MgO 0.1 – 2 Impurity; generally low
TiO₂ 0.1 – 0.5 Impurity; source dependent
SO₃ < 0.1 Sulfate content; generally low
Loss on Ignition (LOI) < 1.4 Indicator of calcination completeness

Note: Na₂O content may vary between different metakaolin sources. Typical metakaolin products generally contain 0.1-0.5% Na₂O. Please refer to the supplier's data for specific product specifications.

4. PHYSICAL PROPERTIES

Property Value Description
Mean Particle Size (D50) ~8 – 10 µm Finely ground; finer than cement
D10 (Particle Distribution) ~1.8 µm Very fine fraction
D90 (Particle Distribution) ~23 µm Coarser fraction
Bulk Density 350 – 600 kg/m³ Loose state; higher when compacted
Specific Gravity ~2400 kg/m³ True density
Moisture Content < 0.1 % Very low; depends on storage conditions
Color Grey – light brown Dependent on source and calcination temperature
Fineness (Blaine) 800 – 1200 m²/kg High specific surface compared to cement
pH (suspension) 5.5 – 7.5 Near neutral in aqueous environment
Thermal Conductivity 0.1 – 0.2 W/mK Low; suitable for insulation applications

5. POZZOLANIC ACTIVITY MECHANISM

5.1. Reaction Mechanism

Metakaolin reacts with calcium hydroxide [Ca(OH)₂] formed during cement hydration to produce additional binding products. This reaction is known as the pozzolanic reaction.

General Reaction:

Metakaolin (SiO₂ + Al₂O₃) + Ca(OH)₂ + H₂O → C-S-H + C-A-H
                                    (Calcium-Silicate-Hydrate)
                                    (Calcium-Aluminate-Hydrate)

Reaction Stages:

Stage Description
1. Hydration Ca(OH)₂ is released during cement hydration
2. Activation Amorphous silica and alumina of metakaolin react with Ca(OH)₂
3. Binder Formation C-S-H (calcium-silicate-hydrate) and C-A-H (calcium-aluminate-hydrate) phases are formed
4. Densification Secondary products improve pore structure

5.2. Pozzolanic Activity Tests

Test Method Value Description
ASTM C618 Class N (Natural Pozzolan) Metakaolin meets the criteria
Calcium Hydroxide Consumption 1000 – 1500 mg Ca(OH)₂/g metakaolin Indicates high activity
Lime Activity > 1,000 psi (7 days) Per ASTM C311

6. PERFORMANCE ENHANCEMENTS

6.1. Mechanical Properties

Performance Parameter Value Description
Compressive Strength Increase (7 days) 15 – 25% Compared to cement-free reference
Compressive Strength Increase (28 days) 20 – 30% More pronounced in the long term
Flexural Strength Increase 10 – 20% Improved flexibility and tensile strength
Modulus of Elasticity 5 – 15% increase More rigid concrete

6.2. Durability Properties

Performance Parameter Value Description
Sulfate Resistance Significant improvement 50-70% more resistant to sulfate attack
ASR Control (Alkali-Silica Reaction) Severe expansion reduction 70-90% reduction in ASR expansion
Chloride Diffusion 60 – 80% lower permeability Protection against reinforcement corrosion
Freeze-Thaw Resistance 95 – 99% durability factor Per ASTM C666
Carbonation Resistance Improved Surface carbonation slows down
Abrasion Resistance 15 – 25% increase Improved surface hardness
Permeability (Chloride) < 1000 Coulombs ASTM C1202 (28 days)

7. APPLICATION AREAS (DETAILED)

7.1. Cement and Concrete Systems (Primary Application)

Application Function Details
High Performance Concrete Pozzolanic admixture Improves strength, durability, and workability
Precast Concrete Early strength enhancer Used to achieve high strength at 7 days
Chemical Resistant Concrete Sulfate and acid resistance Wastewater treatment plants, sewer structures
Silica Fume Alternative Economic alternative Similar performance to silica fume at lower cost
White Cement Color stabilization Preferred in light-colored concretes
Marine Structures Chloride permeability reduction Durability in coastal and marine structures

7.2. Mortar and Plaster Systems

Application Function Details
Repair Mortars Strength enhancer Structural repair and restoration
Plaster Adhesion and strength Improves surface quality
Adhesive Mortars Bond strength Ceramic and tile adhesives
Waterproofing Mortars Impermeability Sealing and water insulation
Self-Leveling Mortar Flowability and strength Floor screeds

7.3. Geopolymer and Alternative Binder Systems

Application Function Details
Geopolymer Production Reactive binder Alkali-activated metakaolin geopolymer synthesis
Cement-Free Binders Carbon footprint reduction Alternative to traditional cement
Impermeable Coatings Surface protection Chemical resistant coatings
Inorganic Polymers High temperature resistance Refractory applications

7.4. Ceramics Industry

Application Function Details
Ceramic Plasticizer Rheological modifier Improves pressing and casting quality
Whitening Agent Color lightening Provides whiteness in ceramic bodies
Glaze Component Matt and opaque effect In ceramic glazes
Refractory Materials Heat resistance High temperature applications
Porcelain Sintering aid Densification and strength

7.5. Polymer and Plastics Industry

Application Function Details
PVC Cable Sheaths Acid scavenger and insulation additive Improves electrical insulation
Polymer Composites Filler and reinforcement Improves mechanical properties
Thermoplastics Melt flow modifier Improves processability
Elastomers Reinforcing filler Improves hardness and abrasion resistance
Coatings Barrier properties Reduces gas and moisture permeability

7.6. Paints and Coatings

Application Function Details
Pigment and Filler Opacity and coverage Improves paint quality
Anti-Corrosion Coatings Barrier effect Protection for metal surfaces
Fire Retardant Coatings Heat barrier Reduces flame spread
Powder Coatings Flowability improvement More uniform coating
Water-Based Paints Viscosity modifier Application ease

7.7. Oil and Gas Industry

Application Function Details
Cement Sheaths Sulfate resistance Well cementing
Mud Stabilization Rheological modifier Drilling muds
Impermeable Barriers Sealing Underground storage

8. DOSAGE AND USAGE RECOMMENDATIONS

Application Recommended Dosage Description
Concrete Admixture 5 – 15% by weight of cement 10-15% for high durability; 5-10% for workability
Mortar Admixture 10 – 20% by weight of cement For repair mortars and adhesives
Geopolymer 70 – 100% (as binder) With alkali activator
Ceramics 1 – 10% by weight Depends on product type
PVC 5 – 15% by weight Cable sheath applications
Paint 5 – 30% by weight As filler and pigment

9. WATER DEMAND AND WORKABILITY

Parameter Value Description
Water/Cement Ratio Increase +2 – 5% Water demand increases with metakaolin use
Superplasticizer Requirement Recommended Workability maintained with superplasticizer
Slump Loss 5 – 15% Workability time may shorten
Concrete Density +1 – 3% More dense concrete

10. STANDARDS AND COMPLIANCE

Standard Description
ASTM C618 Meets Class N (Natural Pozzolan) or Class F (Fly Ash) requirements
ASTM C1709 Standard specification for metakaolin
EN 450 Similar to fly ash standards
EN 13263 Similar performance to silica fume
TS 25 Turkish Cement Standard (as pozzolanic admixture)
ASTM C311 Test methods for pozzolanic activity

11. PACKAGING AND STORAGE

Parameter Information
Packaging Options 15 kg kraft bags, 40 lb bags, 450-2000 kg big-bags
Storage Conditions Store in a dry, cool place away from direct sunlight in original packaging
Shelf Life 24 months under proper conditions; must be kept away from moisture
Moisture Sensitivity High; should be used promptly after opening
Caking May cake in humid environments; sieving recommended before use

12. SAFETY AND TOXICOLOGY

Parameter Information
Acute Oral Toxicity (LD50) > 5,000 mg/kg (low toxicity)
Skin Irritation Mild irritant; prolonged contact should be avoided
Eye Irritation Mild irritant; dust contact may cause mechanical irritation
Inhalation Dust inhalation may cause respiratory tract irritation; long-term exposure carries silicosis risk
Carcinogenicity Not classified as a carcinogen
Water Solubility Insoluble; disperses in water
WGK Germany 1 (low hazard to water)

13. GHS CLASSIFICATION

Hazard Class Category H-Statement
Serious Eye Damage Category 2 H319: Causes serious eye irritation
Specific Target Organ Toxicity (Single Exposure) Category 3 H335: May cause respiratory irritation

Signal Word: WARNING

Hazard Pictograms: GHS07 (Exclamation Mark)

Hazard Statements (H-Codes):

Code Statement
H319 Causes serious eye irritation
H335 May cause respiratory irritation

14. PRECAUTIONARY STATEMENTS (P-CODES)

Code Statement
P261 Avoid breathing dust/fume/gas/mist/vapors/spray
P264 Wash hands thoroughly after handling
P271 Use only outdoors or in a well-ventilated area
P280 Wear protective gloves/protective clothing/eye protection/face protection
P304+P340 IF INHALED: Remove person to fresh air and keep comfortable for breathing
P305+P351+P338 IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses if present
P337+P313 If eye irritation persists: Get medical advice/attention
P501 Dispose of contents/container in accordance with local regulations

15. FIRST AID MEASURES

Route of Exposure Action to Be Taken
Inhalation Move to fresh air. If breathing difficulty occurs, administer oxygen. If symptoms persist, seek medical attention
Skin Contact Wash with plenty of soap and water. Remove contaminated clothing. If irritation develops, seek medical attention
Eye Contact Rinse immediately with plenty of water for at least 15 minutes. Keep eyelids open. If irritation persists, seek medical attention
Ingestion Rinse mouth. If conscious, drink water. Do not induce vomiting. Seek medical attention

16. PHYSICAL AND CHEMICAL HAZARDS

Parameter Information
Flash Point Not applicable (not flammable)
Autoignition Not applicable
Explosive Properties Not explosive
Oxidizing Properties Not oxidizing
Fire Extinguishing Use extinguishing media appropriate to surrounding environment

17. ENVIRONMENTAL INFORMATION

Parameter Information
Aquatic Toxicity Low toxicity; large quantities may have physical effects
Biodegradability Not biodegradable (mineral)
Bioaccumulation Not expected
Environmental Precautions Prevent dry material from entering soil or water
WGK Germany 1 (low hazard to water)

18. REGULATORY STATUS

Region / Authority Status
USA (FDA) Suitable for use in food contact materials
European Union (REACH) Registered
Turkey (KKDIK) Compliance required
OSHA Regulated as dust (respiratory irritation)

19. COMPARATIVE PERFORMANCE TABLE

Property Metakaolin Silica Fume Fly Ash (Class F) Cement (Portland)
Specific Surface (m²/kg) 800-1200 15,000-30,000 300-600 300-400
Pozzolanic Activity High Very High Moderate-High -
Water Demand Moderate High Low Baseline
Early Strength High Very High Low-Moderate Baseline
Sulfate Resistance High High Moderate Low
ASR Control High High Moderate Low
Permeability Very Low Very Low Low High
Cost Moderate High Low Baseline

20. FREQUENTLY ASKED QUESTIONS (FAQ)

Q1: What is metakaolin?

A: Metakaolin is a finely powdered mineral admixture with high pozzolanic activity, obtained by calcining kaolinite mineral (Al₂Si₂O₅(OH)₄) at 600-900°C.

Q2: What is metakaolin's role in cement?

A: Metakaolin reacts with calcium hydroxide [Ca(OH)₂] formed during cement hydration to produce additional C-S-H (calcium-silicate-hydrate). This increases concrete strength, durability, and impermeability.

Q3: What is the difference between metakaolin and silica fume?

A: Silica fume has higher specific surface area (>15,000 m²/kg) and higher pozzolanic activity. However, metakaolin is more economical, has lower water demand, and is advantageous in terms of color (suitable for lighter colored concretes).

Q4: What proportions should metakaolin be used in?

A: 5-15% by weight of cement. 10-15% is preferred for high durability applications, and 5-10% for workability-focused applications.

Q5: How does metakaolin affect water demand?

A: Due to its high specific surface area, metakaolin increases water demand by 2-5%. Therefore, the use of superplasticizer is recommended to maintain workability.

Q6: Which standards does metakaolin comply with?

A: Metakaolin can be used in compliance with ASTM C618 (Class N), ASTM C1709, EN 450, and TS 25 standards.

Q7: What is the shelf life of metakaolin?

A: It is stable for 12 months in its original packaging under proper storage conditions (dry, cool, away from direct sunlight). Once opened, it should be used promptly to prevent moisture absorption.

Q8: Is metakaolin safe?

A: Metakaolin is a mineral admixture with low toxicity. However, inhalation of dust may cause respiratory tract irritation. Use of dust mask, protective goggles, and gloves is recommended during use.

21. QUICK REFERENCE TABLE

Property Value
CAS Number 15123-81-6
Chemical Formula Al₂O₇Si₂
Molecular Weight ~222 g/mol
Appearance Grey – light brown powder
Mean Particle Size (D50) ~8-10 µm
Specific Gravity ~2400 kg/m³
Bulk Density 350-600 kg/m³
Moisture Content < 0.1%
Specific Surface (Blaine) 800-1200 m²/kg
Pozzolanic Activity (7 days) > 1,000 psi
Main Components SiO₂ (50-63%), Al₂O₃ (19-35%)
Loss on Ignition (LOI) < 1.4%
Color Grey – light brown
Shelf Life 24 months (under proper storage)
GHS Signal Word WARNING
UN Number Not applicable
WGK Germany 1 (low hazard to water)

22. CRITICAL NOTICES AND BEST PRACTICES

CRITICAL NOTICES:

  1. Moisture Sensitivity: Metakaolin is sensitive to moisture. Caking and activity loss may occur if the packaging is opened and exposed to moisture. Opened packages should be used immediately or stored in moisture-proof containers.

  2. Dust Control: Metakaolin is a fine particulate material. Inhalation of dust may cause respiratory tract irritation. Long-term exposure carries silicosis risk. Use a dust mask (N95/FFP2) during handling.

  3. Water Demand: Metakaolin increases water demand due to its high specific surface area. Use of superplasticizer is recommended to maintain workability.

  4. Dosage Optimization: Recommended dosages (5-15%) are starting points. Optimum dosage for each application should be determined through trial mixes. Overdosing may cause workability issues and economic inefficiency.

  5. Setting Time: Metakaolin may affect the setting time of cement. Shortening or lengthening of setting time may occur, especially at high dosages (≥10%). This should be monitored through trial mixes.

  6. Color Effect: Metakaolin imparts a light grey-brown color to concrete. Should be used with caution in white or light-colored concretes.

BEST PRACTICE RECOMMENDATIONS:

Concrete Applications:

  • Metakaolin should be mixed dry with cement or added separately to the concrete mixer

  • Use with superplasticizer to maintain workability

  • Water/cement ratio should be optimized

  • Concrete curing should be given care (at least 7 days)

Storage:

  • Store in a dry, cool, well-ventilated place

  • Protect from direct sunlight and moisture

  • Keep tightly closed in original packaging

  • Opened packages should be used promptly

Handling:

  • Use dust mask (N95/FFP2), protective goggles, and gloves

  • Avoid dust formation

  • Use in well-ventilated areas

  • Wash hands after handling

Testing:

  • Conduct trial mixes before application

  • Determine optimum dosage

  • Check setting time and workability

  • Adjust superplasticizer amount if needed

LEGAL DISCLAIMER

This Technical Data Sheet (TDS) is for informational purposes only and is prepared based on available technical data. The user is solely responsible for determining the suitability of the product for their specific application and for complying with all local, national, and international regulations. For complete safety, storage, handling, transport, waste, and regulatory compliance information, the official Safety Data Sheet (SDS/MSDS) provided by the manufacturer/supplier must be consulted. This document does not substitute professional advice. Dosage and application conditions should be optimized through product-specific trials. Chemical composition values are average values and may vary by product grade/quality. Na₂O content may vary by source; please check the supplier's data.

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