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Tannase, Tannin Acyl Hydrolase, Tannin Degrading Enzyme, 9025-56-3

Tannase, Tannin Acyl Hydrolase, Tannin Degrading Enzyme, 9025-56-3

TANNASE (TANNAZ / TANNIN ACYL HYDROLASE)

Tannase / Tannaz / Tannin Acyl Hydrolase / Tannin-Degrading Enzyme
CAS Number: 9025-56-3
EC Number: 3.1.1.20

SECTION 1: PRODUCT IDENTIFICATION AND CHEMICAL IDENTITY

Parameter Information
Product Name Tannase (Tannaz / Tannin Acyl Hydrolase)
Other Names Tannaz, Tannin Acyl Hydrolase, Tannin-Degrading Enzyme, Tanninase
CAS Number 9025-56-3
EC Number 3.1.1.20
Enzyme Class Hydrolase (enzyme that breaks ester bonds)
Source Microbial fermentation (typically Aspergillus oryzaeAspergillus nigerPenicillium species, or Rhizopus species)
Appearance Light brown to beige powder or liquid enzyme preparation
Odor Slight characteristic odor
Physical State (20°C) Solid (powder) or liquid

Tannase (Tannin Acyl Hydrolase) is an enzyme that catalyzes the hydrolysis of ester bonds in hydrolyzable tannins. It converts tannins into simpler compounds such as gallic acid and glucose. It is widely used in the tea, coffee, wine, and juice industries to reduce astringency and bitterness, improve clarity, and enhance flavor profiles. It is also used in the leather industry for tannin removal processes.

SECTION 2: SYNONYMS AND OTHER NAMES

Type Name
Common Names Tannase, Tannaz, Tanninase
Systematic Name Tannin Acyl Hydrolase
EC Number 3.1.1.20
CAS Number 9025-56-3
HS Code 3507.90

SECTION 3: CHEMICAL STRUCTURE

3.1. Molecular Structure

Tannase is a hydrolase enzyme that specifically cleaves ester bonds in hydrolyzable tannins. It is typically a single polypeptide chain with a molecular weight of approximately 60-70 kDa, depending on the microbial source.

Structural Features:

        N-Terminus
            |
    [Catalytic Domain]
            |
    [Substrate Binding Domain]
            |
        C-Terminus

3.2. Key Structural Features

Feature Description
Molecular Weight ~60-70 kDa
Structure Single polypeptide chain
Active Site Serine hydrolase active site
Optimal pH 5.0 – 6.5
Optimal Temperature 30 – 50°C
Substrate Hydrolyzable tannins (gallotannins, ellagitannins)

3.3. Reaction Mechanism

Tannase catalyzes the hydrolysis of ester bonds in gallotannins and ellagitannins, releasing gallic acid and glucose from gallotannins, and ellagic acid from ellagitannins.

General Reaction:

Gallotannin + H₂O → Gallic Acid + Glucose
Ellagitannin + H₂O → Ellagic Acid + Glucose

Hydrolyzable Tannin Breakdown:
Tannin → Gallic Acid + Ellagic Acid + Glucose

SECTION 4: PHYSICAL AND CHEMICAL PROPERTIES

Property Value
Appearance Light brown to beige powder or liquid
Odor Slight characteristic odor
Solubility Soluble in water
Optimal pH Range 5.0 – 6.5
Effective pH Range 4.0 – 7.5
Optimal Temperature 30 – 50°C
Effective Temperature Range 20 – 60°C
Inactivation Temperature >65°C
Stability More stable at neutral pH and low temperatures
Moisture Content (Powder) ≤ 8%
Ash Content ≤ 2%
Heavy Metals ≤ 10 ppm

SECTION 5: ENZYMATIC ACTIVITY

Parameter Value
Activity Definition One unit (U) is defined as the amount of enzyme that liberates 1 µmol of gallic acid per minute at pH 5.5 and 40°C using tannic acid as substrate.
Typical Activity Varies by manufacturer (typically 10,000 – 100,000 U/g or U/mL)
Substrate Hydrolyzable tannins (gallotannins, ellagitannins)
Reaction Products Gallic acid, ellagic acid, glucose

SECTION 6: MECHANISM OF ACTION

Step Description
1 Tannase binds to hydrolyzable tannins (gallotannins or ellagitannins).
2 The enzyme recognizes and binds to ester bonds between gallic acid units and the glucose core.
3 Hydrolysis of the ester bond occurs.
4 Gallic acid (or ellagic acid) and glucose are released.
5 The tannin structure is broken down, reducing astringency and bitterness.

SECTION 7: APPLICATIONS AND INDUSTRIAL USES

7.1. Tea and Coffee Industry

Application Function
Tea Production Reduces astringency and bitterness by breaking down tannins
Instant Tea Improves solubility and clarity
Green Tea Enhances flavor profile and reduces bitter aftertaste
Black Tea Improves color and flavor stability
Coffee Extraction Balances aroma profile
Instant Coffee Improves solubility and reduces astringency
Cold Brew Tea/Coffee Reduces bitterness for improved cold brew products

7.2. Wine and Beer Production

Application Function
Wine Clarification Improves clarity by breaking down tannin-protein complexes
Flavor Improvement Provides a softer taste profile by breaking down tannins
Beer Production Reduces tannin content for improved flavor stability
Cider Production Reduces tannin content for improved flavor

7.3. Fruit Juice Processing

Application Function
Juice Clarification Reduces turbidity and improves clarity
Flavor Enhancement Reduces bitterness and improves taste
Shelf Life Extension Improves stability and extends shelf life
Grape Juice Stabilizes color and flavor

7.4. Leather Industry

Application Function
Tannin Removal Used in tannin removal processes during leather production
Bating Auxiliary in leather processing

7.5. Other Applications

Application Function
Gallic Acid Production Used in the production of gallic acid
Wastewater Treatment Treatment of tannin-rich wastewaters
Animal Feed Improves digestibility of tannin-rich feeds
Cosmetics Used in some skin care formulations

SECTION 8: TYPICAL DOSAGE GUIDELINES

Application Recommended Dosage Conditions
Tea Production 0.01 – 0.1% on tea solids 40-50°C, pH 5.0-5.5
Coffee Extraction 0.02 – 0.1% on coffee solids 40-50°C, pH 5.0-5.5
Wine Clarification 0.01 – 0.05% on wine volume 20-30°C, pH 5.0-6.0
Juice Processing 0.01 – 0.05% on juice volume 30-40°C, pH 5.0-5.5
Beer Production 0.01 – 0.05% on wort volume 20-30°C, pH 5.0-6.0

Note: Dosage should be optimized for each specific application through trial runs.

SECTION 9: PROCESSING GUIDELINES

Parameter Recommendation
Addition Method Dissolve in water and add to the product
Optimal Temperature 30-50°C
Optimal pH 5.0-6.5
Reaction Time 15 minutes to 24 hours (depending on substrate and enzyme concentration)
Inactivation Heat treatment (>65°C) or pH adjustment to inactivate the enzyme
Storage Temperature Store at 4-25°C; for long-term storage, 4°C is recommended

SECTION 10: FACTORS AFFECTING ACTIVITY

Factor Effect
Temperature Optimal at 30-50°C; activity decreases above 60°C; >65°C inactivation
pH Optimal at pH 5.0-6.5; significant activity at pH 4.0-7.5
Substrate Concentration Activity increases with substrate concentration up to saturation
Inhibitors Heavy metals (Cu²⁺, Hg²⁺, Pb²⁺) may inhibit activity
Tannin Type Hydrolyzable tannins are preferred substrates over condensed tannins
Stability More stable at neutral pH and low temperatures

SECTION 11: TOXICOLOGICAL PROFILE

Parameter Value
Acute Oral Toxicity (LD50, Rat) > 5,000 mg/kg (very low toxicity)
Acute Dermal Toxicity Low
Acute Inhalation Toxicity May cause respiratory sensitization (dust)
Skin Irritation Mild irritant
Eye Irritation May cause mild irritation
Skin Sensitization May cause sensitization in sensitive individuals
Mutagenicity Negative (Ames test)
Carcinogenicity Not classified as a carcinogen
Reproductive Toxicity Not classified as a reproductive toxin
Allergenicity May cause allergic reactions in sensitive individuals (protein-based)

SECTION 12: GHS CLASSIFICATION

Hazard Class Category H-Statement
Respiratory Sensitization Category 1 H334
Skin Sensitization Category 1 H317

Signal Word: WARNING

Hazard Pictograms: GHS07 (Exclamation Mark), GHS08 (Health)

Hazard Statements (H-Codes):

Code Statement
H317 May cause an allergic skin reaction.
H334 May cause allergy or asthma symptoms or breathing difficulties if inhaled.

SECTION 13: PRECAUTIONARY STATEMENTS (P-CODES)

Code Statement
P261 Avoid breathing dust/fume/gas/mist/vapors/spray.
P264 Wash hands thoroughly after handling.
P271 Use only outdoors or in a well-ventilated area.
P280 Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352 IF ON SKIN: Wash with plenty of soap and water.
P304+P340 IF INHALED: Remove person to fresh air and keep comfortable for breathing.
P305+P351+P338 IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses if present.
P342+P311 If experiencing respiratory symptoms: Call a POISON CENTER/doctor.
P333+P313 If skin irritation or rash occurs: Get medical advice/attention.
P337+P313 If eye irritation persists: Get medical advice/attention.
P362+P364 Take off contaminated clothing and wash it before reuse.
P501 Dispose of contents/container in accordance with local regulations.

SECTION 14: FIRST AID MEASURES

Route of Exposure Action to Be Taken
Inhalation Move to fresh air. If respiratory irritation persists, seek medical attention.
Skin Contact Wash with plenty of soap and water. Remove contaminated clothing. If irritation persists, consult a physician.
Eye Contact Rinse thoroughly with plenty of water for at least 15 minutes. Remove contact lenses. If irritation persists, seek medical attention.
Ingestion Rinse mouth with water. Drink plenty of water. Do not induce vomiting. If large amount is swallowed, seek medical attention.

SECTION 15: FIRE-FIGHTING MEASURES

Parameter Information
Fire Hazard Combustible organic powder; may burn at high temperatures.
Hazards During Fire Thermal decomposition produces toxic fumes including carbon monoxide, carbon dioxide, and nitrogen oxides.
Suitable Extinguishing Media Water spray, CO₂, dry chemical powder, alcohol-resistant foam.
Special Protective Equipment Self-contained breathing apparatus (SCBA), full protective clothing.

SECTION 16: ACCIDENTAL RELEASE MEASURES

Parameter Information
Personal Protection Dust mask, protective goggles, gloves, coverall.
Ventilation Increase ventilation; use local exhaust in confined spaces.
Containment Cover spilled area to prevent dust dispersion.
Cleaning Methods Collect dry using vacuum or careful sweeping. Avoid washing with water (soluble).
Environmental Precautions Prevent entry into drains, sewers, and water bodies.
Waste Disposal Dispose of in accordance with local regulations.

SECTION 17: STORAGE AND SHELF LIFE

Parameter Information
Storage Conditions Store in a cool, dry, and well-ventilated area at 4-25°C.
Long-Term Storage 4°C is recommended for long-term storage.
Container Requirements Keep tightly closed in original packaging. Protect from moisture and direct sunlight.
Materials to Avoid Strong oxidizers, high heat, moisture.
Shelf Life 12 months (in unopened original packaging under proper storage).
Stability Note Enzyme activity decreases over time; store at recommended temperatures to maintain activity.
Packaging Options Aluminum foil bags, plastic containers.

SECTION 18: PACKAGING OPTIONS

Packaging Type Quantity Material
Aluminum Foil Bag 1 kg Laminated aluminum
Plastic Container 1 kg, 5 kg, 10 kg HDPE / Food-grade plastic
Fiber Drum 25 kg Cardboard / Plastic

SECTION 19: TRANSPORT INFORMATION

Parameter Information
UN Number Not applicable (not classified as dangerous goods)
Hazard Class Not classified as hazardous for transport
Packing Group Not applicable
ADR/RID Not regulated
IMDG Code Not regulated
IATA (Air) Not regulated
Marine Pollutant No
Transport Temperature Ambient temperature; protect from moisture.

SECTION 20: REGULATORY INFORMATION

Region / Authority Status
European Union Approved as a food enzyme (EU 1332/2008).
USA (FDA) GRAS (Generally Recognized as Safe) for food applications.
Turkey Approved as a food processing aid (Turkish Food Codex).
EFSA Re-evaluated and considered safe at current usage levels.
Kosher/Halal Can be certified upon request.

SECTION 21: ENVIRONMENTAL INFORMATION

Parameter Information
Aquatic Toxicity Low toxicity to aquatic organisms.
Biodegradability Readily biodegradable (protein-based).
Bioaccumulation Not expected.
Waste Disposal Dispose of in accordance with local regulations. Incineration is recommended for contaminated materials.

SECTION 22: COMPARISON WITH OTHER ENZYMES

Property Tannase Pectinase Xylanase Protease
Substrate Tannins Pectin Xylan Proteins
Bond Cleaved Ester bonds (tannins) α-1,4 glycosidic bonds β-1,4 glycosidic bonds Peptide bonds
Optimal pH 5.0-6.5 4.0-6.0 4.5-6.0 6.0-8.0
Optimal Temperature 30-50°C 40-55°C 40-60°C 40-60°C
Primary Application Tea, coffee, wine Juice, wine Baking, paper, biofuel Baking, dairy, meat

SECTION 23: FREQUENTLY ASKED QUESTIONS (FAQ)

Q1: What is tannase used for?
A: Tannase is used to break down tannins in tea, coffee, wine, and fruit juices. It reduces astringency and bitterness, improves clarity, and enhances the flavor profile of beverages.

Q2: Is tannase safe to eat?
A: Yes. Tannase is considered safe (GRAS by FDA, approved by EFSA) for food applications. The enzyme is inactivated during processing and is not present in the final product.

Q3: What is the optimal pH and temperature for tannase?
A: The optimal pH is 5.0-6.5, and the optimal temperature is 30-50°C. The enzyme is inactivated above 65°C.

Q4: Can tannase be used in wine production?
A: Yes. Tannase is used in wine production to reduce astringency, improve clarity, and enhance flavor stability.

Q5: How should tannase be stored?
A: Store in a cool, dry place at 4-25°C, in tightly closed original packaging. For long-term storage, 4°C is recommended. Protect from moisture and direct sunlight.

SECTION 24: QUICK REFERENCE TABLE

Property Value
CAS Number 9025-56-3
EC Number 3.1.1.20
Molecular Weight ~60-70 kDa
Appearance Light brown to beige powder or liquid
Solubility Soluble in water
Optimal pH 5.0 – 6.5
Optimal Temperature 30 – 50°C
Inactivation Temperature >65°C
Primary Substrate Hydrolyzable tannins (gallotannins, ellagitannins)
Primary Uses Tea, coffee, wine, juice processing
Shelf Life 12 months
UN Number Not applicable
GHS Signal Word WARNING

SECTION 25: CRITICAL NOTICES AND BEST PRACTICES

CRITICAL NOTICES:

  1. CAS Number Verification: The correct CAS number for tannase (tannin acyl hydrolase) is 9025-56-3. This enzyme should not be confused with xylanase (CAS 9025-57-4).

  2. Respiratory Sensitization: Tannase powder may cause respiratory sensitization (H334) in susceptible individuals. Use appropriate dust control measures and respiratory protection.

  3. Skin Sensitization: May cause allergic skin reactions (H317) in sensitive individuals. Use protective gloves.

  4. Enzyme Activity: Enzyme activity decreases with temperature, pH, and time. Optimize conditions for each application to achieve desired results.

  5. Heat Inactivation: The enzyme is inactivated above 65°C. This ensures that no active enzyme remains in the final product after processing.

  6. Dosage Optimization: Recommended dosages are starting points. Conduct trial runs to optimize the dosage for specific applications and products.

  7. Substrate Specificity: Tannase is most effective on hydrolyzable tannins (gallotannins, ellagitannins). It is less effective on condensed tannins.

  8. Storage: Store at recommended temperatures (4-25°C). For long-term storage, 4°C is recommended. Higher temperatures accelerate activity loss.

  9. Flavor Impact: Overdosing may cause excessive hydrolysis and undesirable flavor changes. Optimize dosage for the desired flavor profile.

BEST PRACTICE RECOMMENDATIONS:

  • Storage: Store in a cool, dry, and well-ventilated area at 4-25°C. For long-term storage, 4°C is recommended. Keep containers tightly closed. Protect from moisture and direct sunlight.

  • Handling: Use dust mask, protective gloves, and goggles. Avoid dust formation. Ensure adequate ventilation.

  • Dissolution: Dissolve in water at room temperature. Use immediately after dissolution.

  • Application: Add the enzyme to the product at the appropriate stage of processing. Ensure uniform distribution.

  • Incubation: Allow sufficient reaction time at the optimal temperature for the enzyme to act. Reaction time varies by application.

  • Inactivation: Ensure the final product is heated to >65°C or pH-adjusted to inactivate the enzyme.

  • Dosage: Start with recommended dosages and optimize through trial runs. Overdosing may cause excessive hydrolysis and undesirable flavor changes.

  • Quality Control: Monitor enzyme activity and product quality regularly. Test for residual enzyme activity if required.

  • Waste Management: Dispose of waste in accordance with local regulations.

LEGAL DISCLAIMER:

This Technical Data Sheet (TDS) is for informational purposes only and is prepared based on available technical data. The user is solely responsible for determining the suitability of the product for their specific application and for complying with all local, national, and international regulations. For complete safety, storage, handling, transport, waste, and regulatory compliance information, the official Safety Data Sheet (SDS/MSDS) provided by the manufacturer/supplier must be consulted. This document does not substitute professional advice. Dosage and application conditions should be optimized through product-specific trials. The CAS number for tannase is 9025-56-3; this should not be confused with xylanase (CAS 9025-57-4).

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