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Isophthalic Acid, Benzene Dicarboxylic Acid, PIA, IPA, 121-91-5

Isophthalic Acid, Benzene Dicarboxylic Acid, PIA, IPA, 121-91-5

ISOPHTHALIC ACID (PIA)

Isophthalic Acid / Benzene-1,3-dicarboxylic Acid / PIA / IPA
CAS Number: 121-91-5
EC Number: 204-506-4

SECTION 1: PRODUCT IDENTIFICATION AND CHEMICAL IDENTITY

Parameter Information
Product Name Isophthalic Acid
Abbreviation PIA / IPA
Chemical Name (IUPAC) Benzene-1,3-dicarboxylic Acid
Other Names Isophthalic Acid, 1,3-Benzenedicarboxylic Acid, m-Phthalic Acid
CAS Number 121-91-5
EC Number (EINECS) 204-506-4
Molecular Formula C₆H₄(CO₂H)₂ / C₈H₆O₄
Molecular Weight 166.13 g/mol
Chemical Class Aromatic dicarboxylic acid
Appearance White crystalline powder
Odor Practically odorless
Physical State (20°C) Solid (crystalline)

Isophthalic Acid is an aromatic dicarboxylic acid with the carboxyl groups positioned at the 1,3- (meta) positions on the benzene ring. It is a versatile intermediate used primarily in the production of high-performance unsaturated polyester resins, alkyd resins, and various engineering plastics. Compared to terephthalic acid and phthalic anhydride, isophthalic acid offers superior properties such as improved chemical resistance, thermal stability, and mechanical strength.

SECTION 2: SYNONYMS AND OTHER NAMES

Type Name
Common Names Isophthalic Acid, PIA, IPA
Chemical Names Benzene-1,3-dicarboxylic Acid, 1,3-Benzenedicarboxylic Acid, m-Phthalic Acid
CAS Number 121-91-5
EC Number 204-506-4
HS Code 2917.39

SECTION 3: CHEMICAL STRUCTURE

3.1. Molecular Structure

Isophthalic acid consists of a benzene ring with two carboxyl groups (-COOH) attached at the 1 and 3 positions (meta configuration).

Structural Formula:

        COOH
         |
         C
        / \
       /   \
      /     \
     /       \
    C         C
    |         |
    C - H     C - COOH
    |         |
    C         C
     \       /
      \     /
       \   /
        \ /
         C
          \
           COOH

Simplified Representation:

        COOH
         |
    C₆H₄ - COOH
    (1,3-configuration)

3.2. Molecular Formula

C₆H₄(CO₂H)₂ / C₈H₆O₄

3.3. Molecular Weight

166.13 g/mol

3.4. Key Structural Features

Feature Description
Core Structure Benzene ring (C₆H₄)
Functional Groups Two carboxyl groups (-COOH)
Substitution Pattern 1,3 (meta) configuration
Aromatic Ring 6-membered ring with delocalized electrons
Acidity Dicarboxylic acid (two acidic protons)

SECTION 4: PHYSICAL AND CHEMICAL PROPERTIES

Property Value
Appearance White crystalline powder
Odor Practically odorless
Molecular Formula C₆H₄(CO₂H)₂ / C₈H₆O₄
Molecular Weight 166.13 g/mol
Density ~1.54 g/cm³
Melting Point ~345 °C
Boiling Point Sublimes (decomposes before boiling)
Water Solubility (20°C) Low (~0.1 g/L)
Solubility in Methanol Slightly soluble
Solubility in Acetone Slightly soluble
Solubility in Ethanol Slightly soluble
Solubility in Dimethylformamide (DMF) Soluble
Solubility in Dimethyl Sulfoxide (DMSO) Soluble
pKa₁ (25°C) ~3.54
pKa₂ (25°C) ~4.60
Flash Point Non-flammable (solid)
Autoignition Temperature ~650 °C
Stability Stable under normal storage conditions

SECTION 5: SOLUBILITY PROFILE

Solvent Solubility Conditions
Water Low (~0.1 g/L) 20°C
Water Slightly soluble 100°C
Methanol Slightly soluble 25°C
Ethanol Slightly soluble 25°C
Acetone Slightly soluble 25°C
Dimethylformamide (DMF) Soluble 25°C
Dimethyl Sulfoxide (DMSO) Soluble 25°C
Benzene Insoluble 25°C
Toluene Insoluble 25°C

SECTION 6: CHEMICAL PROPERTIES AND REACTIVITY

Property Description
Chemical Character Weakly acidic (dicarboxylic acid)
Stability Stable under normal storage conditions
Reactivity Reacts with alcohols to form esters; with amines to form amides
Esterification Reacts with alcohols to produce isophthalate esters
Polycondensation Reacts with glycols to form polyesters
Decomposition Decomposes at high temperatures to CO₂ and benzene derivatives
Incompatible Materials Strong oxidizers, strong bases, reducing agents

SECTION 7: REACTION EQUATIONS

7.1. Esterification with Alcohols

PIA + 2 R-OH → Isophthalate Diester + 2 H₂O

7.2. Polyester Formation with Glycols

PIA + HO-R-OH → Polyester + H₂O

7.3. Neutralization with Bases

PIA + 2 NaOH → Sodium Isophthalate + 2 H₂O

7.4. Amidation with Amines

PIA + 2 R-NH₂ → Isophthalamide + 2 H₂O

SECTION 8: PRODUCTION METHOD

Isophthalic Acid is produced primarily by the oxidation of m-xylene.

Stage Process Description
1 Oxidation m-Xylene is oxidized in the liquid phase with air in the presence of a catalyst (cobalt/manganese/ bromine system) at elevated temperature and pressure.
2 Separation The crude isophthalic acid is separated from the reaction mixture.
3 Purification The crude product is purified by recrystallization or distillation to obtain high-purity isophthalic acid.
4 Drying The purified product is dried to remove residual moisture.
5 Packaging The dried product is packaged in appropriate containers.

Overall Reaction:
m-Xylene + 3 O₂ → Isophthalic Acid + 2 H₂O

SECTION 9: APPLICATIONS AND INDUSTRIAL USES

9.1. Polyester Resins (Most Important Application)

Application Description
Unsaturated Polyester Resins (UPR) Provides high chemical resistance, thermal stability, and mechanical strength
High-Performance Polyesters Used in corrosion-resistant applications (tanks, pipes, marine)
Sheet Molding Compounds (SMC) Automotive parts, construction panels
Bulk Molding Compounds (BMC) Electrical components, appliance parts

9.2. Coatings and Paints

Application Description
Alkyd Resins Provides hardness, gloss, and weather resistance
Powder Coatings Provides excellent weatherability and chemical resistance
Industrial Coatings High-performance coatings for metal and wood
Automotive Coatings Provides durability and gloss retention

9.3. Plastic Additives

Application Description
Plasticizers Isophthalate esters as non-phthalate plasticizers
Heat Stabilizers Thermal stabilizer for PVC
Flame Retardants Intermediate for flame retardant compounds

9.4. Engineering Plastics

Application Description
Polyurethanes Rigid and flexible foams
Polyamide-imides High-performance engineering plastics
Polybenzimidazoles High-temperature polymers

9.5. Adhesives and Sealants

Application Description
Adhesive Formulations Provides adhesion and durability
Structural Adhesives High-strength bonding applications

9.6. Other Applications

Application Description
Fiberglass Reinforced Plastics Marine, automotive, construction
Paints and Varnishes High-quality finishes
Electrical Insulation Insulating materials
Printing Inks Specialty ink formulations

SECTION 10: ISOPHTHALIC ACID VS. OTHER PHTHALIC ACIDS

Property Isophthalic Acid (PIA) Terephthalic Acid (PTA) Phthalic Anhydride (PA)
Substitution Pattern 1,3 (meta) 1,4 (para) 1,2 (ortho, anhydride)
Melting Point ~345°C ~300°C 131.6°C
Solubility Low Very low Hydrolyzes
Chemical Resistance Excellent Excellent Moderate
Thermal Stability Excellent Excellent Moderate
Applications UPR, coatings, adhesives PET, fibers, bottles Plasticizers, UPR

SECTION 11: TOXICOLOGICAL PROFILE

Parameter Value
Acute Oral Toxicity (LD50, Rat) > 5,000 mg/kg (low toxicity)
Acute Dermal Toxicity (LD50, Rabbit) > 2,000 mg/kg
Acute Inhalation Toxicity Low risk; dust may cause respiratory irritation
Skin Irritation Mild irritant (powder)
Eye Irritation Moderate irritant (powder)
Skin Sensitization Not a sensitizer
Mutagenicity Negative
Carcinogenicity Not classified as a carcinogen
Reproductive Toxicity Not classified as a reproductive toxin
Target Organs No specific target organs identified

SECTION 12: GHS CLASSIFICATION

Hazard Class Category H-Statement
Eye Irritation Category 2 H319
Skin Irritation Category 2 H315
Specific Target Organ Toxicity - SE Category 3 H335

Signal Word: WARNING

Hazard Pictograms: GHS07 (Exclamation Mark)

Hazard Statements (H-Codes):

Code Statement
H315 Causes skin irritation.
H319 Causes serious eye irritation.
H335 May cause respiratory irritation.

SECTION 13: PRECAUTIONARY STATEMENTS (P-CODES)

Code Statement
P261 Avoid breathing dust.
P264 Wash hands thoroughly after handling.
P271 Use only outdoors or in a well-ventilated area.
P280 Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352 IF ON SKIN: Wash with plenty of soap and water.
P305+P351+P338 IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses if present.
P337+P313 If eye irritation persists: Get medical advice/attention.
P501 Dispose of contents/container in accordance with local regulations.

SECTION 14: FIRST AID MEASURES

Route of Exposure Action to Be Taken
Inhalation Move to fresh air. If respiratory irritation persists, seek medical attention.
Skin Contact Wash with plenty of soap and water. Remove contaminated clothing. If irritation persists, consult a physician.
Eye Contact Rinse thoroughly with plenty of water for at least 15 minutes. Remove contact lenses. If irritation persists, seek medical attention.
Ingestion Rinse mouth with water. Drink plenty of water. Do not induce vomiting. If large amount is swallowed, seek medical attention.
General Note If symptoms persist, always consult a healthcare facility.

SECTION 15: FIRE-FIGHTING MEASURES

Parameter Information
Fire Hazard Combustible organic solid; may burn at high temperatures.
Hazards During Fire Thermal decomposition produces carbon monoxide and carbon dioxide.
Suitable Extinguishing Media Water spray, CO₂, dry chemical powder, alcohol-resistant foam.
Special Protective Equipment Self-contained breathing apparatus (SCBA), full protective clothing.

SECTION 16: ACCIDENTAL RELEASE MEASURES

Parameter Information
Personal Protection Dust mask, protective goggles, gloves, coverall.
Ventilation Increase ventilation; use local exhaust in confined spaces.
Containment Cover spilled area to prevent dust dispersion.
Cleaning Methods Collect dry using vacuum or careful sweeping. Avoid washing with water.
Environmental Precautions Prevent entry into drains, sewers, and water bodies.
Waste Disposal Dispose of in accordance with local regulations.

SECTION 17: STORAGE AND SHELF LIFE

Parameter Information
Storage Conditions Store in a cool, dry, and well-ventilated area at room temperature (15-25°C).
Container Requirements Keep tightly closed in original packaging. Protect from moisture.
Materials to Avoid Strong oxidizers, strong bases, reducing agents.
Shelf Life 24 months (under proper storage conditions).
Stability Note Stable; protect from moisture to prevent caking.
Packaging Options 25 kg bags, 500 kg big-bags, 1000 kg palletized.

SECTION 18: PACKAGING OPTIONS

Packaging Type Quantity Material
Kraft Bag + PE Liner 25 kg Paper / Polyethylene
Plastic Drum 25 kg HDPE
Fiber Drum 25 kg Cardboard / Plastic
Big-Bag 500 – 1000 kg Polypropylene

SECTION 19: TRANSPORT INFORMATION

Parameter Information
UN Number Not applicable (not classified as dangerous goods)
Hazard Class Not classified as hazardous for transport
Packing Group Not applicable
ADR/RID Not regulated
IMDG Code Not regulated
IATA (Air) Not regulated
Marine Pollutant No
Transport Temperature Ambient temperature; protect from moisture.

SECTION 20: REGULATORY INFORMATION

Region / Authority Status
European Union (REACH) Registered; industrial chemical.
USA (TSCA) Listed.
Turkey (KKDIK) Registered under chemical registration regulations.
EINECS 204-506-4
FDA Indirect food contact approved (certain grades)

SECTION 21: ENVIRONMENTAL INFORMATION

Parameter Information
Aquatic Toxicity Low toxicity to aquatic organisms
Biodegradability Slowly biodegradable
Bioaccumulation Low potential
Mobility in Soil Low to moderate
Waste Disposal Incineration or disposal in accordance with local regulations

SECTION 22: OTHER NAMES AND SYNONYMS

Name Context
Isophthalic Acid Common name
PIA Abbreviation
IPA Abbreviation
Benzene-1,3-dicarboxylic Acid IUPAC name
1,3-Benzenedicarboxylic Acid Chemical name
m-Phthalic Acid Chemical name
CAS 121-91-5
EC 204-506-4

SECTION 23: QUICK REFERENCE TABLE

Property Value
CAS Number 121-91-5
EC Number 204-506-4
Molecular Formula C₆H₄(CO₂H)₂ / C₈H₆O₄
Molecular Weight 166.13 g/mol
Appearance White crystalline powder
Odor Practically odorless
Density ~1.54 g/cm³
Melting Point ~345 °C
Water Solubility (20°C) Low (~0.1 g/L)
Primary Uses Polyester resins, coatings, adhesives, engineering plastics
Shelf Life 24 months
UN Number Not applicable
GHS Signal Word WARNING

SECTION 24: CRITICAL NOTICES AND BEST PRACTICES

CRITICAL NOTICES:

  1. Dust Hazard: Isophthalic acid is a fine powder that can form dust clouds. Avoid inhalation and dust formation. Use local exhaust ventilation.

  2. Moisture Sensitivity: Protect from moisture to prevent caking and agglomeration.

  3. Thermal Stability: Stable at room temperature; decomposes at high temperatures.

  4. Incompatibility: Incompatible with strong oxidizers, strong bases, and reducing agents.

  5. Eye and Skin Irritation: May cause irritation. Use appropriate personal protective equipment.

  6. Quality Grades: Various grades available (standard, high-purity, polymer grade). Select appropriate grade for your application.

BEST PRACTICE RECOMMENDATIONS:

  • Storage: Store in a cool, dry, and well-ventilated area. Keep containers tightly closed. Protect from moisture.

  • Handling: Use protective gloves, goggles, and dust mask. Avoid dust formation. Ensure adequate ventilation.

  • Processing: In polyester resin production, use appropriate catalysts and reaction conditions.

  • Quality Control: Test for purity, moisture content, and color. Ensure product meets specifications.

  • Waste Management: Dispose of waste in accordance with local regulations. Incineration is recommended for contaminated materials.

LEGAL DISCLAIMER:

This Technical Data Sheet (TDS) is for informational purposes only and is prepared based on available technical data. The user is solely responsible for determining the suitability of the product for their specific application and for complying with all local, national, and international regulations. For complete safety, storage, handling, transport, waste, and regulatory compliance information, the official Safety Data Sheet (SDS/MSDS) provided by the manufacturer/supplier must be consulted. This document does not substitute professional advice.

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