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Aerosil R 202, Hydrophobic Silica, Fumed Silica, Pyrogenic Silica, 68909-20-6

Aerosil R 202, Hydrophobic Silica, Fumed Silica, Pyrogenic Silica, 68909-20-6

AEROSIL R 202

SECTION 1: PRODUCT IDENTITY AND CHEMICAL IDENTIFICATION

Parameter Information
Product Name Aerosil R 202
Chemical Description Surface-modified amorphous silica (hydrophobized with organic silane)
CAS Number 68909-20-6
EINECS Number 272-697-1
Molecular Structure Amorphous SiO₂
Chemical Class Hydrophobic fumed silica (pyrogenic silica)
Surface Modification Organic silane (polydimethylsiloxane)
Physical State (20°C) Solid (fine powder)
Color White
Odor Odorless
Type Hydrophobic

SECTION 2: CHEMICAL STRUCTURE

Structure Description:

              O
              ‖
    —Si—O—Si—O—Si—
      |     |     |
      O     O     O
      |     |     |
    —Si—O—Si—O—Si—
      |     |     |
     CH₃   CH₃   CH₃
      |     |     |
     Si     Si     Si
      |     |     |
    …CH₃   …CH₃   …CH₃

    Aerosil R 202
    Amorphous silica (SiO₂) network surface-modified
    with organic silane (polydimethylsiloxane)

Simplified Structure:

    SiO₂ (Amorphous) — Surface Modification: —Si(CH₃)₃ groups

    Aerosil R 202
    Hydrophobic Fumed Silica
Parameter Description
Base Material Fumed (pyrogenic) silica (SiO₂)
Surface Modification Treated with polydimethylsiloxane (PDMS)
Surface Property Hydrophobic
Surface Groups -Si(CH₃)₃ (trimethylsilyl)
Surface Area (BET) ~100-130 m²/g
Primary Particle Size 7-14 nm
Agglomerate Size ~1-10 μm
Tapped Density ~50-70 g/L
pH (4% Aqueous Dispersion) 4.0 – 6.0

SECTION 3: PHYSICAL AND CHEMICAL PROPERTIES

Property Value Test Method / Note
Appearance White, fine powder Visual
Odor Odorless Olfactometric
SiO₂ Content ≥99.0% Gravimetric
Tapped Density ~50-70 g/L ASTM D4164
True Density ~2.2 g/cm³ -
Surface Area (BET) 100-130 m²/g DIN 66131
Primary Particle Size 7-14 nm TEM / SEM
Agglomerate Size ~1-10 μm Laser Diffraction
pH (4% Aqueous Dispersion) 4.0 – 6.0 DIN EN ISO 787-9
Loss on Drying (105°C) ≤1.0% Gravimetric
Loss on Ignition (1000°C) ≤4.0-6.0% Gravimetric
Carbon Content ~2.0-4.0% Elemental Analysis
Hydrophobicity Hydrophobic (water-repellent) Test
Water Solubility Insoluble General Method
Dispersion in Organic Solvents Dispersible (liquid oils, esters, alcohols) General Method
Flash Point >200°C -
Melting Point >1000°C (glass melting) -
Optical Properties Transparentizing -
Dusting Low (hydrophobic) -

SECTION 4: AEROSIL GRADES COMPARISON

Property Aerosil R 202 Aerosil 200 Aerosil R 972 Aerosil 300
Surface Property Hydrophobic Hydrophilic Hydrophobic Hydrophilic
Surface Area (BET) 100-130 m²/g 175-225 m²/g 90-130 m²/g 300-350 m²/g
Modification PDMS None DDS None
Carbon Content ~2-4% None ~1-2% None
Primary Particle (nm) 7-14 12 16 7
pH (4% Aqueous) 4.0-6.0 3.8-4.5 3.8-5.0 3.8-4.5
Tapped Density (g/L) ~50 ~50 ~50 ~50
Main Application Cosmetics, pharmaceuticals, oily systems General purpose, water-based Epoxy, oily systems High viscosity, film
Hydrophobicity High Low High Low

SECTION 5: FUNCTIONAL PROPERTIES

Property Description
Thickener Increases viscosity in formulations; Provides non-Newtonian flow behavior; High rheological effect at low concentrations.
Emulsifier Stabilizes oil-water emulsions; Prevents emulsion separation; Reduces surfactant requirements.
Rheology Control Regulates flow properties; Provides thixotropic behavior; Application ease and flow control.
Flow Regulator Improves flowability in powder formulations; Prevents caking and sticking; Acts as lubricant and glidant in tablet production.
Hydrophobicity Water-repellent property; Dispersibility in organic systems; Effectiveness in oily formulations.
Transparentizing Agent Improves optical properties; Reduces cloudiness; Provides transparency in film-forming systems.

SECTION 6: MAIN APPLICATION AREAS

Industry / Application Function Typical Concentration
Cosmetics (Creams, Lotions) Thickener, emulsifier, rheology control 0.5-5%
Cosmetics (Makeup, Sunscreens) Thickener in oily systems, water resistance 0.5-3%
Pharmaceutical (Tablets) Flow regulator, glidant, lubricant 0.1-1%
Pharmaceutical (Capsules) Flow regulator, anti-adherent 0.1-1%
Pharmaceutical (Topical Creams) Thickener, emulsion stabilizer 0.5-3%
Food Additive Flow regulator, anti-caking agent 0.1-1%
Paints and Coatings Rheology control, viscosity adjustment 0.5-5%
Adhesives and Sealants Thickener, flow control 0.5-3%
Epoxy and Resin Systems Rheology control, sag resistance 0.5-3%
Spray and Aerosol Suspension stabilizer 0.5-2%

SECTION 7: FORMULATION GUIDELINES

Parameter Recommendation
Concentration Typical concentration: 0.5-5% (depending on formulation)
Addition Method Dispersion with high-speed mixing; Recommended to add at final stage; Disperse using three-roll mill or high-shear mixer.
Dispersion Medium Dispersible in oily systems (mineral oil, esters, silicone oils, triglycerides); Not dispersible in water; Dispersible in organic solvents.
pH Range Stable in pH 4.0 – 9.0; Stable in acidic and basic environments.
Temperature Resistance Stable from -20°C to +200°C; Avoid prolonged exposure at high temperatures.
Activation Pre-wetting recommended; High effect even at low concentrations; Activated by high shear force.
Compatibility Compatible with most organic components; Compatible with polymers, oils, resins, solvents; Thixotropic effect at high concentrations.
Synergistic Effects Combination with other hydrophobic silicas (Aerosil R 972); Use with organo-clays, polymers; Synergy with viscosity enhancers.
Dust Control Should be used to minimize dust formation; Well-ventilated area; Dust mask recommended.

SECTION 8: SAMPLE FORMULATIONS

Skin Cream (For Oily Skin):

Component Quantity
Aerosil R 202 1.0%
Water 75.0%
Oil Phase (liquid oils, emulsifiers) 20.0%
Preservatives, Fragrance As required

Instructions: Add to oil phase; Disperse with high-speed mixing; Emulsify with water phase; Homogenize.

Tablet Flow Regulator (Pharmaceutical):

Component Quantity
Aerosil R 202 0.2-0.5%
Active Ingredient As required
Excipients (Filler, Binder) As required

Instructions: Add during final mixing stage; Ensure homogeneous blend; Direct compression or granulation.

SECTION 9: QUALITY SPECIFICATIONS

Parameter Specification Test Method
Appearance White, fine powder Visual
SiO₂ Content ≥99.0% Gravimetric
Surface Area (BET) 100-130 m²/g DIN 66131
Primary Particle Size 7-14 nm TEM / SEM
pH (4% Aqueous Dispersion) 4.0 – 6.0 DIN EN ISO 787-9
Loss on Drying (105°C) ≤1.0% Gravimetric
Loss on Ignition (1000°C) ≤4.0-6.0% Gravimetric
Carbon Content ~2.0-4.0% Elemental Analysis
Tapped Density 50-70 g/L ASTM D4164
Hydrophobicity Hydrophobic Test
Heavy Metals (Pb) ≤10 ppm ICP-MS
Arsenic (As) ≤2 ppm ICP-MS
Lead (Pb) ≤3 ppm ICP-MS
Cadmium (Cd) ≤1 ppm ICP-MS
Mercury (Hg) ≤1 ppm ICP-MS
Microbiological Purity TAMC ≤10² CFU/g; TYMC ≤10¹ CFU/g USP <61>
E. coli Negative in 1g USP <62>
Salmonella spp. Negative in 25g USP <62>

SECTION 10: SAFETY PROFILE AND TOXICOLOGICAL ASSESSMENT

Parameter Value / Description
GHS Classification Not classified as hazardous substance
Signal Word None (not hazardous)
Hazard Pictograms None
Hazard Statements (H-Codes) None
Acute Oral Toxicity (LD50, Rat) >5000 mg/kg (low toxicity)
Acute Inhalation Toxicity Dust inhalation may cause irritation
Skin Irritation Not irritant
Eye Irritation May cause mild irritation (mechanical)
Skin Sensitization Does not cause sensitization
Carcinogenicity Not classified as carcinogenic
Mutagenicity Not mutagenic
Reproductive Toxicity No reproductive toxicity
Target Organs Respiratory tract (dust)
Occupational Exposure Limit 4 mg/m³ (8-hour TWA)
Systemic Toxicity Low
Ecology Insoluble in water; Low toxicity

SECTION 11: GHS CLASSIFICATION AND LABELING

GHS Classification (in accordance with 1272/2008/EC):

Hazard Class Category H-Statement
Not classified as hazardous substance

Signal Word: None (Not classified as hazardous)

Hazard Pictograms: None

NFPA 704 Hazard Classification:

Health Flammability Reactivity Special
1 0 0 -
(Minimal health hazard) (Non-combustible) (Stable) (None)

SECTION 12: PRECAUTIONARY STATEMENTS (P-CODES)

Code Statement
P261 Avoid breathing dust/fume/gas
P264 Wash hands thoroughly after handling
P271 Use only outdoors or in a well-ventilated area
P280 Wear protective gloves/protective clothing/eye protection/face protection
P304+P340 IF INHALED: Remove person to fresh air and keep comfortable for breathing
P305+P351+P338 IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses if present and continue rinsing
P403+P233 Store in a well-ventilated place. Keep container tightly closed
P501 Dispose of contents/container in accordance with local/regional/national/international regulations

SECTION 13: FIRST AID MEASURES

Route of Exposure Action
Inhalation If inhaled as powder, move to fresh air. Seek medical attention if respiratory symptoms persist.
Skin Contact Remove contaminated clothing. Wash with plenty of soap and water. Seek medical attention if irritation develops.
Eye Contact Rinse thoroughly with plenty of water for at least 15 minutes. Keep eyelids open. Remove contact lenses if present. Seek medical attention if irritation persists.
Ingestion Rinse mouth with water. Do NOT induce vomiting. Drink 1-2 glasses of water. Seek medical attention.
Note Symptomatic treatment is administered. No specific antidote available.

SECTION 14: FIREFIGHTING MEASURES

Parameter Information
Fire Hazard Non-combustible. Remains as inert powder at high temperatures.
Fire-Related Hazards No thermal decomposition products (inorganic).
Suitable Extinguishing Media Water mist, CO₂, dry chemical powder, foam.
Unsuitable Extinguishing Media Water jet (may spread dust)
Special Protective Equipment Self-contained breathing apparatus (SCBA), full protective clothing.
Special Precautions Prevent dust from entering sewers and water bodies.

SECTION 15: STORAGE AND SHELF LIFE

Parameter Information
Storage Conditions Store in a cool, dry, well-ventilated area; protect from direct sunlight and moisture.
Temperature Limits 15-25°C (ideal); do not exceed 30°C
Humidity Low humidity environment
Light No light protection required
Container Requirements Tightly closed, moisture-resistant containers (PE-lined bags, HDPE containers)
Incompatible Materials Strong alkalis, hydrofluoric acid
Shelf Life 24-36 months (unopened original packaging, under proper storage conditions)
Shelf Life (After Opening) 12-24 months (under proper storage conditions)
Signs of Degradation Caking, moisture absorption (loss of hydrophobicity), reduced flowability
Stability Warning Stable under normal conditions; Hydrophobicity may decrease over time in high humidity

SECTION 16: PACKAGING OPTIONS

Packaging Type Quantity / Capacity Material Application Area
PE-Lined Kraft Bag 10 kg, 20 kg Kraft paper / PE liner Industrial supply
Multi-layer Paper Bag 10 kg, 20 kg Paper (air and moisture-proof) Industrial, food
HDPE Drum 10 kg, 20 kg HDPE (opaque, moisture barrier) Pharmaceutical, cosmetic
Aluminum Foil Bag 1 kg, 5 kg Aluminum / PE (moisture-proof) High purity, pharmaceutical
IBC Container 500 kg, 1000 kg UV-protected HDPE Large-scale industrial supply

SECTION 17: TRANSPORTATION INFORMATION

Parameter Information
UN Number Not applicable (not classified as dangerous substance)
Hazard Class Not applicable
Packing Group Not applicable
ADR/RID Not classified as dangerous goods
IMDG Code Not marine pollutant
IATA (Air) Not classified as dangerous goods; can be transported by air
Transport Temperature Ambient temperature; protect from moisture
Transport Precautions Moisture-proof packaging
Spill Cleanup Collect mechanically; clean with absorbent material; avoid dust generation
Marine Pollutant No

SECTION 18: REGULATORY STATUS

Region / Authority Status
USA (FDA) GRAS (21 CFR 182.1711); Approved as food additive
USA (EPA) Listed as inert ingredient
European Union (EC) Approved as food additive (E551)
Turkey Approved as food additive, pharmaceutical and cosmetic excipient; Subject to KKDIK regulation
ECHA (REACH) Registered substance
TSCA (USA) Listed
California (Prop 65) Not listed
Halal Yes (synthetic, not animal-derived)
Kosher Yes (with certification)
Vegan Yes (synthetic)

SECTION 19: OTHER NAMES AND SYNONYMS

Type Name
Turkish Names Aerosil R 202, Hidrofobik Silika, Fumed Silika
English Names Aerosil R 202, Hydrophobic Silica, Fumed Silica, Pyrogenic Silica
CAS Number 68909-20-6
EINECS Number 272-697-1
E Number E551 (food additive)
HS Code 2811.22

SECTION 20: SUMMARY TABLE

Parameter Value
CAS Number 68909-20-6
Chemical Structure Amorphous SiO₂ (surface-modified)
Appearance White, fine powder
Surface Property Hydrophobic
Surface Area (BET) 100-130 m²/g
Primary Particle Size 7-14 nm
pH (4% Aqueous) 4.0 – 6.0
SiO₂ Content ≥99.0%
Primary Function Thickener, emulsifier, rheology control, flow regulator
Main Applications Cosmetics, pharmaceuticals, food, industrial
Shelf Life 24-36 months
Storage Cool, dry, air-tight
GHS Classification Not hazardous
UN Number Not applicable
FDA Status GRAS (21 CFR 182.1711)
Halal / Kosher / Vegan Yes

SECTION 21: CRITICAL WARNINGS AND BEST PRACTICES

CRITICAL WARNINGS:

  1. Dust Control: Should be used to minimize dust formation. Airborne dust concentrations may cause respiratory irritation.

  2. Hydrophobicity: Water-repellent; does not disperse in water-based systems. Should only be dispersed in oily and organic systems.

  3. Dispersion: Requires high shear force for dispersion; low shear force results in insufficient dispersion.

  4. Storage: Must be protected from moisture; moisture may reduce hydrophobicity.

  5. Temperature: Avoid prolonged exposure at high temperatures (>200°C).

  6. Incompatible Materials: Do not contact with strong alkalis (NaOH, KOH) and hydrofluoric acid (HF).

BEST PRACTICE RECOMMENDATIONS:

  1. Concentration: Typical concentration 0.5-5%; adjust according to desired viscosity.

  2. Addition Method: Add during final stage of formulation; disperse with high-speed mixing.

  3. Pre-dispersion: Pre-wetting improves dispersion; wet in oil phase.

  4. High Shear: Use three-roll mill or high-shear mixer for dispersion.

  5. pH Control: Stable in pH 4.0-9.0; stable in acidic and basic environments.

  6. Synergy: Can be used with other hydrophobic silicas or organo-clays.

  7. Personal Protective Equipment: Dust mask (N95/FFP2), safety goggles, protective clothing.

  8. Hygiene: Wash hands thoroughly after handling; Do not eat, drink or smoke when using this product.

  9. Quality Control: Regularly perform surface area (BET), pH, loss on drying, carbon content, microbiological purity tests.

  10. Storage: Store in cool, dry, air-tight containers. Keep tightly closed after opening.

LEGAL DISCLAIMER:

The information provided in this document is based on our current knowledge and experience and is presented in good faith. However, as all conditions of use are beyond our control, it does not constitute a binding specification or guarantee. This Technical Data Sheet is for informational purposes only. Users are responsible for testing suitability for their own applications and for complying with all local, regional, and national regulations. For complete safety, storage, use, handling, waste, and regulatory compliance information, please refer to the official Safety Data Sheet (SDS/MSDS) provided by the manufacturer/supplier.

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