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Vanillyl Butyl Ether, Butyl Vanillyl Ether, VBE, 82654-98-6

Vanillyl Butyl Ether, Butyl Vanillyl Ether, VBE, 82654-98-6

VANILLYL BUTYL ETHER (VANIL BUTIL ETER)

Vanillyl Butyl Ether / 4-(Butoxymethyl)-2-methoxyphenol / Butyl Vanillyl Ether
CAS Number: 82654-98-6
FEMA Number: 3796

1. PRODUCT IDENTIFICATION AND CHEMICAL IDENTITY

Parameter Detail
Product Name Vanillyl Butyl Ether
Chemical Name (IUPAC) 4-(Butoxymethyl)-2-methoxyphenol
Other Names Vanil Butyl Ether, Butyl Vanillyl Ether, 2-Methoxy-4-(butoxymethyl)phenol, VBE
CAS Number 82654-98-6
EINECS Number 209-753-1
Molecular Type Aromatic ether derivative
Molecular Formula C₁₂H₁₈O₃
Molecular Weight 210.27 g/mol
MDL Number MFCD00238529
Appearance Colorless to pale yellow liquid
Odor Mild vanilla-like aroma, creamy vanilla notes

Vanillyl Butyl Ether is an ether derivative of vanillyl alcohol and n-butanol. It is a synthetic sensory ingredient used in cosmetic and personal care products to provide a warming (thermogenic) effect. When applied to the skin, it activates TRPV1 (Vanilloid Receptor-1) channels, generating a sensation of warmth, which increases blood circulation and creates a soothing effect. It is widely used in cosmetics, personal care products, and topical pharmaceutical preparations.

2. SYNONYMS AND OTHER NAMES

Type Name
Common Names Vanillyl Butyl Ether, Vanil Butyl Ether, Butyl Vanillyl Ether
Chemical Names 4-(Butoxymethyl)-2-methoxyphenol, 2-Methoxy-4-(butoxymethyl)phenol
Abbreviations VBE
FEMA Number 3796
CAS Number 82654-98-6
EINECS Number 209-753-1
HS Code 2909.50.4050

3. CHEMICAL STRUCTURE

3.1. Molecular Structure

Vanillyl Butyl Ether is a vanillin alcohol derivative containing a methoxy group (-OCH₃) and a butoxymethyl side chain (-CH₂-O-C₄H₉) on the phenolic ring.

Structural Formula:

        OH
         |
         C
        / \
       /   \
      /     \
     /       \
    C         C
    |         |
    H         C - H
    |         |
    C - O - CH₂ - O - (CH₂)₃ - CH₃
    |         |
    H         C - H
    |         |
    C         C
    |         |
    H         O - CH₃

SMILES Notation:
CCCCOCC1=CC(OC)=C(O)C=C1

3.2. Molecular Formula

C₁₂H₁₈O₃

3.3. Molecular Weight

210.27 g/mol

3.4. Key Structural Features

Feature Description
Functional Groups Phenolic hydroxyl (-OH), Methoxy (-OCH₃), Ether (-O-), Aromatic ring
Aroma Class Vanilla, spicy
Chemical Class Aromatic ether derivative
TRPV1 Activity Activates TRPV1 receptor through vanilloid structure

4. PHYSICAL AND CHEMICAL PROPERTIES

Property Value / Description
Appearance Colorless to pale yellow liquid
Odor Mild vanilla-like, creamy vanilla aroma
Molecular Weight 210.27 g/mol
Boiling Point 241 °C
Density (25°C) 1.057 g/mL
Refractive Index n²⁰/D 1.516 (literature)
Flash Point >230 °F (>110 °C)
Vapor Pressure 0.42-2000 Pa (20-25°C)
LogP 2.2-2.4 (23-25°C)
Water Solubility ~1.79-1690 mg/L (20°C)
Solubility Soluble in oils and organic solvents; insoluble in water
Stability Sensitive to oxidation; should be stored under inert atmosphere

5. SOLUBILITY PROFILE

Solvent Solubility Conditions
Water Insoluble 20°C
Vegetable Oils Soluble 25°C
Ethanol Soluble 25°C
Organic Solvents Soluble 25°C

6. CHEMICAL PROPERTIES AND REACTIVITY

Property Description
Chemical Character Weakly acidic (phenolic OH group)
Oxidation Sensitive to oxidation in air; inert atmosphere recommended
Heat Sensitivity May decompose at high temperatures
Incompatible Materials Strong oxidizers, strong bases

7. MECHANISM OF ACTION (THERMOGENIC EFFECT)

Parameter Description
TRPV1 Activation Vanillyl Butyl Ether activates TRPV1 (Vanilloid Receptor-1) channels due to its vanilloid structure. These receptors are ion channels that respond to stimuli such as high temperature and acidic pH.
Neuronal Activation Receptor activation leads to the release of glutamate, ATP, and various neuropeptides from neurons.
Warm Sensation This process creates a long-lasting and mild warmth sensation on the skin.
Blood Circulation The thermogenic effect increases blood circulation in the application area.

8. APPLICATIONS AND INDUSTRIAL USES

8.1. Cosmetics and Personal Care (Most Important Application)

Application Description Typical Usage Rate
Massage Creams Provides muscle-relaxing and soothing warmth sensation 1 – 5%
Sports Gels Warming effect for pre- and post-exercise use 1 – 5%
Warming Lotions Used in body warmers and slimming products 1 – 5%
Foot Care Products Warming and soothing foot creams 1 – 5%
Hair Care Products Provides sensory effect on the scalp 0.5 – 2%

8.2. Pharmaceutical Topical Preparations

Application Description
Heating Ointments Topical preparations that provide warmth sensation for muscle and joint pain
Pain Relief Gels Mild analgesic and soothing effect
Veterinary Products Anti-emetic dietary compositions for pets

8.3. Flavor and Fragrance Industry

Application Description
Food Flavor (FEMA 3796) Provides heating and spicy taste notes in baked goods, confectionery, beverages, chocolate, tea, and mint products
Taste Masking Provides warming sensation in the mouth and masks unwanted tastes

8.4. Other Applications

Application Description
Weight Management Supports metabolism by increasing body temperature in slimming products
Oral Care Oral care formulations that provide a warm sensation in the mouth

9. CHEMICAL COMPATIBILITY TABLE

Substance / Environment Compatibility Description
Water INCOMPATIBLE Insoluble; requires emulsification.
Oils COMPATIBLE Easily miscible.
Ethanol COMPATIBLE Soluble.
Oxidizers INCOMPATIBLE May cause degradation.
Air / Oxygen LIMITED Sensitive to oxidation; inert atmosphere recommended.
Light LIMITED UV light may accelerate degradation.
Heat LIMITED May decompose at high temperatures.

10. TOXICOLOGICAL PROFILE

Parameter Value
Acute Oral Toxicity Low toxicity
Skin Irritation May be irritating at high concentrations
Skin Sensitizer Weak skin sensitizer; NESIL value 3500 μg/cm²
Eye Irritation Causes serious eye irritation (H319)
Genotoxicity Negative
Phototoxicity Negative
Photosensitization Negative
Bioaccumulation Low; not PBT (Persistent, Bioaccumulative, Toxic)
Environmental Risk PEC/PNEC ratio <1 (safe under current use)

11. GHS CLASSIFICATION AND LABELING

GHS Classification:

Hazard Class Category H-Statement
Eye Irritation Category 2 H319
Skin Sensitizer Category 1 H317
Aquatic Toxicity Category 3 H412 (in some notifications)

Signal Word: WARNING

Hazard Pictograms: GHS07 (Exclamation Mark)

Hazard Statements (H-Codes):

Code Statement
H317 May cause an allergic skin reaction.
H319 Causes serious eye irritation.
H412 Harmful to aquatic life with long-lasting effects.

12. PRECAUTIONARY STATEMENTS (P-CODES)

Code Statement
P261 Avoid breathing dust/fume/gas/mist/vapors/spray.
P264 Wash hands thoroughly after handling.
P272 Contaminated work clothing should not be allowed out of the workplace.
P280 Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352 IF ON SKIN: Wash with plenty of soap and water.
P305+P351+P338 IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses if present.
P333+P313 If skin irritation or rash occurs: Get medical advice/attention.
P337+P313 If eye irritation persists: Get medical advice/attention.
P362+P364 Take off contaminated clothing and wash it before reuse.
P501 Dispose of contents/container in accordance with local regulations.

13. FIRST AID MEASURES

Route of Exposure Action to Be Taken
Inhalation Move to fresh air. If breathing difficulty occurs, seek medical attention.
Skin Contact Wash with plenty of soap and water. Remove contaminated clothing. If irritation or rash occurs, seek medical attention.
Eye Contact Rinse thoroughly with plenty of water for at least 15 minutes. Remove contact lenses. Seek medical attention.
Ingestion Rinse mouth with water. Do not induce vomiting. Seek immediate medical attention.

14. FIRE-FIGHTING MEASURES

Parameter Information
Fire Hazard Flammable liquid (Storage Class 10)
Suitable Extinguishing Media Dry chemical powder, CO₂, alcohol-resistant foam, water spray.
Hazards During Fire Thermal decomposition produces carbon monoxide, carbon dioxide, and toxic fumes.
Special Protective Equipment Self-contained breathing apparatus (SCBA), full protective clothing.

15. ACCIDENTAL RELEASE MEASURES

Parameter Information
Personal Protection Protective gloves, goggles, protective clothing.
Ventilation Increase ventilation; use local exhaust in confined spaces.
Containment Cover spilled area with inert material (sand, vermiculite).
Cleaning Methods Collect with inert absorbent material and place in appropriate waste container.
Environmental Precautions Prevent entry into drains, sewers, and water bodies.

16. STORAGE AND SHELF LIFE

Parameter Information
Storage Conditions Store in a cool (below 15°C recommended), dry, and well-ventilated area; protect from light.
Container Requirements Tightly closed, under inert atmosphere (nitrogen), in airtight containers.
Materials to Avoid Light, oxygen, heat, strong oxidizers.
Shelf Life 24 months (under proper storage conditions).
Packaging Options 1 kg, 5 kg, 25 kg (dark-colored glass or aluminum containers).

17. TRANSPORT INFORMATION

Parameter Information
UN Number Not applicable (not classified as dangerous goods).
Hazard Class Not classified as hazardous for transport.
Packing Group Not applicable.
ADR/RID Not classified as dangerous goods.
IMDG Code Not classified as dangerous goods.
IATA (Air) Not classified as dangerous goods.
Transport Temperature Ambient temperature; protect from light and oxygen.

18. REGULATORY STATUS

Region / Authority Status
European Union Approved as cosmetic ingredient (EU 1223/2009).
FDA Approved for use as food additive (FDA 21 CFR 117).
IFRA Can be used in accordance with usage guidelines.
JECFA Meets purity specifications (JECFA No: 888).
REACH Actively registered.
TSCA Listed.
Halal / Kosher May be certified upon request.

19. SECTORAL SUITABILITY TABLE

Sector Suitability Description
Cosmetics HIGH Massage creams, sports gels, warming lotions, hair care.
Personal Care HIGH Thermal effect formulations, foot care products.
Pharmaceuticals MEDIUM Topical heating ointments, pain relief gels.
Food Flavor HIGH Baked goods, confectionery, beverages, chocolate, tea.
Veterinary LOW Pet dietary compositions.

20. QUICK REFERENCE TABLE

Property Value
CAS Number 82654-98-6
Molecular Formula C₁₂H₁₈O₃
Molecular Weight 210.27 g/mol
Appearance Colorless to pale yellow liquid
Odor Mild vanilla-like
Boiling Point 241 °C
Density (25°C) 1.057 g/mL
Refractive Index 1.516
Flash Point >230 °F (>110 °C)
Solubility Soluble in oils; insoluble in water
Main Uses Cosmetics (warming effect), food flavor, topical preparations
Shelf Life 24 months
GHS Warning (H317, H319)
UN Number Not applicable

21. CRITICAL NOTICES AND BEST PRACTICES

CRITICAL NOTICES:

  1. External Use Only: Vanillyl Butyl Ether is for external (topical) use only. Should not be taken orally.

  2. Eye and Mucous Membrane Contact: Avoid contact with eyes and mucous membranes. In case of contact, rinse thoroughly with water and seek medical attention.

  3. Skin Sensitization Potential: May cause an allergic skin reaction (H317). Patch testing is recommended for individuals with sensitive skin.

  4. Irritation at High Concentrations: May cause skin irritation at high concentrations. Recommended usage rates (1-5%) should be followed.

  5. Facial and Eye Area Products: Should not be used in products applied to the face, eye area, or other sensitive body areas.

  6. Oxidation Sensitivity: Sensitive to oxidation; should be stored under inert atmosphere and protected from light.

  7. TRPV1 Mechanism: Due to its vanilloid structure, it activates TRPV1 receptors to generate warmth sensation; this mechanism is similar to capsaicin.

BEST PRACTICE RECOMMENDATIONS:

  • Storage: Store in a cool (below 15°C), dry, and well-ventilated area, under inert atmosphere (nitrogen), in airtight containers. Protect from light.

  • Personnel Protection: Use protective gloves, goggles, and appropriate work clothing.

  • Formulation: Suitable for use in emulsions, creams, and gels. Dissolve in oil phase. Recommended starting concentration is 1-5%.

  • Dosage Control: Do not use in facial and eye area products. Start with low concentrations in sensitive areas.

  • Quality Control: Monitor peroxide value to check for oxidation products.

  • Waste Management: Dispose of waste in accordance with local regulations. Do not pour down drains.

LEGAL DISCLAIMER:

The information provided in this document is based on our current knowledge and experience and is presented in good faith; however, as all conditions of use are beyond our control, it does not constitute a binding specification or warranty. This Technical Data Sheet is for informational purposes only. Users are obligated to test the suitability of the product for their own applications. For complete safety, storage, handling, transport, waste, and regulatory compliance information, the official Safety Data Sheet (SDS/MSDS) provided by the manufacturer/supplier must be consulted.

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