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Calcium Formate, Calcium Diformiate, 544-17-2

Calcium Formate, Calcium Diformiate, 544-17-2

CALCIUM FORMATE (CALCIUM FORMIATE)

Calcium Formate / Calcium Diformate / Formic Acid Calcium Salt
CAS Number: 544-17-2
EC Number: 208-863-7

1. PRODUCT IDENTIFICATION AND CHEMICAL IDENTITY

Parameter Description
Chemical Name (IUPAC) Calcium diformate
Other Names Calcium formate, Calcium diformiate, Formic acid calcium salt
CAS Number 544-17-2
EC Number (EINECS) 208-863-7
Molecular Formula C2H2CaO4
Molecular Weight 130.12 g/mol
Chemical Class Organic carboxylate salt (metal formate)
Appearance White crystalline powder or granules
Odor Slight characteristic, non-acidic odor

Calcium formate is the calcium salt of formic acid. It is an organic compound formed by the bonding of two formate ions (HCOO-) to one calcium cation (Ca2+). Due to its high water solubility and near-neutral pH, it finds widespread use in construction, leather, feed, and industrial chemical sectors. Its most important feature is that it accelerates cement setting without causing steel reinforcement corrosion, as it contains no chlorides. Additionally, in animal nutrition, it serves as an organic acid preservative that supports digestive system health.

2. PHYSICAL AND CHEMICAL PROPERTIES

Property Value
Molecular Formula C2H2CaO4
Molecular Weight 130.12 g/mol
Appearance White crystalline powder or free-flowing granules
Odor Slight characteristic
Density 2.2 g/cm3 (20°C)
Bulk Density 700 – 900 kg/m3
Melting Point Decomposes at 300°C (no distinct melting point)
pH (10% aqueous solution, 20°C) 6.0 – 8.0
Water Solubility (20°C) 160 g/L
Solubility in Organic Solvents Slightly soluble in methanol and ethanol; insoluble in acetone
Hygroscopicity Low; moderate sensitivity to moisture
LogP (Octanol/Water) Negative (hydrophilic)
Toxicity (Oral LD50, Rat) 5000 mg/kg

Calcium formate has high solubility in water (approximately 160 g/L at 20°C) and its aqueous solution is in the neutral pH range. This property allows easy mixing and homogeneous distribution in cement mortars. When heated above 300°C, it decomposes into calcium carbonate, formaldehyde, and water vapor.

3. SOLUBILITY PROFILE

Solvent Solubility Conditions
Water 160 g/L 20°C
Water 200 g/L 50°C
Methanol Slightly soluble 25°C
Ethanol Slightly soluble 25°C
Acetone Insoluble 25°C
Ether Insoluble 25°C

Calcium formate is readily soluble in water but insoluble in most organic solvents. Its solubility in water increases significantly with rising temperature.

4. CHEMICAL PROPERTIES AND REACTIONS

Property Description
Chemical Class Organic salt (carboxylate)
Unique Structure Contains two formate groups bonded to a calcium ion
Acid-Base Properties Weakly basic salt in aqueous solution (pH 6-8)
Thermal Decomposition Decomposes above 300°C into CaCO3, CH2O, and H2O
Oxidation Resistance Reacts with strong oxidizers due to organic structure
Complex Formation Can form stable complexes with metal ions
Incompatible Substances Strong acids (releases formic acid), strong oxidizers

Calcium formate has an ionic character as a metal salt. When dissolved in water, it dissociates into calcium (Ca2+) and formate (HCOO-) ions. Contact with strong acids yields formic acid and calcium salts. It is thermally stable and can be safely used in industrial processes.

5. SPECIFICATIONS (TECHNICAL GRADE)

Parameter Specification
Purity (as Ca(HCOO)2 basis) 98.0%
Moisture (Loss on Drying) 0.5%
pH (10% aqueous solution, 20°C) 6.0 – 8.0
Calcium Oxide (CaO) Content 30.5%
Free Formic Acid Content 0.5%
Chloride (Cl-) 0.05%
Sulfate (SO42-) 0.1%
Heavy Metals (as Pb) 10 ppm
Iron (Fe) 20 ppm
Particle Size (standard) 100% passes through 2 mm sieve
Appearance White, free-flowing crystalline powder

Technical grade Calcium formate is optimized for construction and industrial applications. Its low chloride content minimizes corrosion risk in reinforced concrete applications.

6. APPLICATIONS AND INDUSTRIAL USES

Calcium formate is widely used across various industries due to its low toxicity, chloride-free nature, and high solubility.

6.1. Construction and Cement Industry

Application Description
Setting Accelerator Reduces setting time in cement and mortars, particularly accelerating strength development in cold weather conditions.
Chloride-Free Anti-Freeze Used safely as an alternative to corrosive additives such as calcium chloride.
Flowability Regulator Improves workability of mortar and concrete.
Early Strength Additive Reduces formwork removal time, especially in precast concrete elements.

Calcium formate accelerates cement hydration by interacting with the C3A (tricalcium aluminate) phase, thereby increasing early strength gain of concrete.

6.2. Leather Tanning Industry

Application Description
Neutralization Agent Used to raise the pH of leather after chrome tanning.
Pre-Treatment for Fatliquoring Prepares tanned leather for the fatliquoring process.
pH Buffer Helps maintain the desired pH level in tanning baths.

6.3. Feed Additive (Animal Nutrition)

Application Description
Antibacterial Preservative Inhibits the growth of pathogenic microorganisms, particularly in swine and poultry feeds.
Digestive Regulator Supports intestinal flora and improves digestion.
Organic Acid Source Acts as a source of formic acid in feeds, enhancing feed hygiene.
Performance Enhancer Shown to improve weight gain and feed conversion ratios in animals.

6.4. Industrial Chemistry and Other Applications

Application Description
Formic Acid Production Evaluated as a formic acid source in recycling processes.
Buffer Solutions Used as a pH stabilizer in industrial cleaning and dyeing processes.
Textile Printing Acts as a fixative in textile printing dyes.
De-icing Agent Used in non-corrosive aircraft and runway de-icing formulations.

7. BIOLOGICAL AND STRUCTURAL PROPERTIES

Property Description
Metabolism Metabolized in the body to formic acid and subsequently to CO2 and water.
Calcium Source Provides bioavailable calcium.
Antimicrobial Effect Converts to formic acid at low pH, exhibiting bacteriostatic effects.
Absorption Rapidly absorbed from the digestive tract and excreted via the kidneys.
Toxicity Profile Low systemic toxicity; LC50 1000 mg/L (aquatic organisms)

In animal nutrition, calcium formate hydrolyzes to formic acid in the digestive system. Formic acid penetrates bacterial cell membranes, lowering internal pH and inhibiting microbial growth. It also enhances digestive enzyme activity.

8. BIOCHEMICAL APPLICATIONS

Application Description
Microbiology Studies Used as a carbon and mineral source in bacterial cultures.
Enzyme Studies Serves as a substrate in formate dehydrogenase enzyme studies.
Metabolomics Used as a standard compound in organic acid metabolism research.
Bioremediation Can be used for precipitation of heavy metal ions.

9. SAFETY AND TOXICOLOGY

Parameter Value
GHS Classification Not classified as hazardous
Oral LD50 (Rat) 5000 mg/kg
Dermal LD50 2000 mg/kg (rabbit)
Skin Irritation Not irritating
Eye Irritation May cause mild irritation (in powder form)
Respiratory Irritation Mild irritation upon inhalation of dust
Skin Sensitization Negative
Mutagenicity Negative
Carcinogenicity Not classified
Bioaccumulation Unlikely (LogP negative)
WGK (Germany Water Hazard Class) 1 (slight hazard to water)
Ecotoxicity (Daphnia) EC50 100 mg/L

Calcium formate presents low risk to human health and the environment. However, prolonged exposure to dust may cause respiratory tract irritation. Dust masks and protective goggles are recommended for industrial use.

10. TRANSPORT INFORMATION

Parameter Information
UN Number Not applicable (not hazardous)
Hazard Class Not classified as hazardous
Packing Group Not applicable
Proper Shipping Name Calcium formate
Marine Pollutant No
ADR/RID Label Not applicable
Transport Category Category 0 (no restrictions)
Air Transport (IATA) No restrictions

Calcium formate is not classified as a dangerous good for international transport and can be safely shipped by road, sea, and air.

11. REGULATORY INFORMATION

Region Status
EU (REACH) Registered and commercialized
Turkey (KKDIK) Mandatory compliance; registration process ongoing
USA (TSCA) Listed
FDA Compliance GRAS (Generally Recognized as Safe) as a feed additive
EFSA (European Food Safety Authority) Approved as a feed additive
Turkish Food Codex Permitted for use as a feed additive

Calcium formate is regulated and approved as a feed additive and construction chemical in all major industrial markets, including the EU, USA, Turkey, Japan, and China.

12. STORAGE AND HANDLING

Parameter Information
Storage Conditions Cool, dry, and well-ventilated area; room temperature (15-25°C)
Container Requirements Tightly closed original packaging (25 kg kraft bags)
Materials to Avoid Strong acids, strong oxidizers
Shelf Life 24 months (under proper storage)
Hygroscopicity Low; however, prolonged exposure to moisture may cause caking and loss of flowability
Packaging Options 25 kg bags, 500 kg big-bags, 1000 kg palletized shipment
Handling Notes Avoid dust formation; use local exhaust ventilation; nitrile gloves and protective goggles recommended

Handling Notes:

  • Use closed systems to prevent dust formation.

  • Avoid contact with skin, eyes, and respiratory tract.

  • Reseal packaging tightly after use to protect from moisture.

  • Recommended dosage in cement and mortars is typically 0.5-2.0% of cement weight.

13. FIRE-FIGHTING MEASURES

Parameter Information
Fire Hazard Not flammable, but decomposes at high temperatures
Extinguishing Media Water spray, CO2, dry chemical powder, alcohol-resistant foam
Special Hazards Thermal decomposition produces carbon monoxide, carbon dioxide, and calcium oxide fumes
Protective Equipment Self-contained breathing apparatus (SCBA), full protective clothing
Explosion Risk Does not form explosive mixtures with air

In case of fire, avoid inhaling decomposition products and use full protective equipment.

14. ACCIDENTAL RELEASE MEASURES

Parameter Information
Personal Protection Dust mask, protective goggles, nitrile gloves, coverall
Ventilation Increase ventilation; use local exhaust in confined spaces
Containment Cover spilled area to prevent dust dispersion
Cleaning Methods Collect dry using vacuum or careful sweeping; avoid washing with water (soluble)
Environmental Precautions Prevent entry into drains, sewers, and water bodies
Waste Disposal Dispose of as chemical waste in accordance with local regulations

For large spills, keep the product dry, collect it, and place it in labeled containers for proper disposal.

15. FIRST AID MEASURES

Route of Exposure Action to Be Taken
Inhalation Move person to fresh air. Administer oxygen if breathing difficulty occurs. Seek medical attention.
Skin Contact Wash with plenty of soap and water. Remove contaminated clothing. If irritation persists, consult a physician.
Eye Contact Rinse thoroughly with plenty of water for at least 15 minutes. Keep eyelids open. Remove contact lenses if present. Consult a physician.
Ingestion Rinse mouth. Drink plenty of water. Do not induce vomiting. If unconscious, do not administer anything orally. Seek immediate medical attention.
General Note If symptoms persist, always consult a healthcare facility.

Although calcium formate has low toxicity, precautions should be taken in cases of dust inhalation, eye contact, or skin contact.

16. RAW MATERIALS AND DERIVATIVES

16.1. Raw Materials (Upstream)

Raw Material Description
Formic Acid Main chemical precursor
Calcium Hydroxide (Slaked Lime) Calcium source
Calcium Carbonate (Limestone) Alternative calcium source
Carbon Monoxide / Sodium Formate By-products of formic acid production

16.2. Derivatives (Downstream)

Derivative Application
Formic Acid (Recycling) Acid source in the chemical industry
Calcium Carbonate Result of thermal decomposition; industrial filler material
Calcium Complexes Specialty chemicals and ion exchangers
Concrete Admixture Solutions Liquid formulations for use in ready-mix concrete plants

17. SECTORAL SUITABILITY AND USAGE AMOUNTS

Sector Application Area Example Use Suitability
Construction Concrete and mortar admixture Precast elements, cold-weather concrete Very High
Leather Tanning neutralization pH adjustment of chrome-tanned leather High
Feed Antibacterial preservative Swine and poultry feeds High
Chemicals Buffer and reaction aid Industrial cleaning products Suitable
Agriculture Silage preservative Limited use Limited
Textiles Printing fixative Fabric dyeing processes Suitable

18. CARBON DIOXIDE CAPTURE PROPERTY

Calcium formate is also being evaluated in some industrial processes as a carbon dioxide (CO2) capture agent. In aqueous solutions, calcium ions can bind CO2 by forming carbonate and bicarbonate compounds. This property is being researched, particularly in closed-loop carbon capture systems. However, this application is more niche and experimental compared to the construction and feed sectors.

19. DERIVATIVES AND RELATED COMPOUNDS

Compound Description
Sodium Formate Sodium-based formate salt with similar structure
Potassium Formate Used in liquid de-icing formulations
Calcium Lactate Another organic calcium salt used as food and feed additive
Calcium Acetate Alternative salt used in construction and food sectors
Formic Acid Acidic form of calcium formate; preservative and pH regulator
Calcium Formate (Anhydrous) Moisture-free form for special applications

20. SUMMARY AND CRITICAL NOTICES

SUMMARY:

Calcium formate (C2H2CaO4, CAS 544-17-2) is the calcium salt of formic acid and appears as a white crystalline powder. Its molecular weight is 130.12 g/mol, water solubility at 20°C is approximately 160 g/L, and its aqueous solution has a neutral pH (6-8). It decomposes at 300°C. Its most significant advantage is that it accelerates cement setting without causing corrosion of steel reinforcement due to its chloride-free nature. This makes it an indispensable additive in the construction sector. It is also widely used as a neutralization agent in leather tanning, as an antibacterial preservative in animal nutrition, and as a buffering agent in industrial processes. Its low toxicity, high biodegradability, and environmentally friendly profile make it a safe chemical.

KEY PROPERTIES (Summary Table):

Property Value
Appearance White crystalline powder or granules
Chemical Formula C2H2CaO4
Molecular Weight 130.12 g/mol
CAS Number 544-17-2
Melting Point Decomposes at 300°C
Water Solubility (20°C) 160 g/L
pH (10% aqueous solution) 6.0 – 8.0
Purity 98%
Primary Use Concrete setting accelerator, feed preservative, leather neutralization

MAIN APPLICATION AREAS:

Sector Applications
Construction Setting accelerator, early strength additive, chloride-free anti-freeze
Leather Post-chrome neutralization and pre-fatliquoring preparation
Feed Antibacterial preservative, digestive regulator, performance enhancer
Chemicals Buffer solutions, formic acid source, textile printing fixative

KEY SAFETY POINTS:

  • Low toxicity: Not classified as hazardous; LD50 5000 mg/kg.

  • Non-irritating: No skin irritation; mild eye irritation possible in powder form.

  • Non-mutagenic/non-carcinogenic: No carcinogenic classification.

  • Storage: 15-25°C, cool, dry, tightly closed, away from moisture.

  • PPE recommended: Dust mask (P2), protective goggles, nitrile gloves.

  • Incompatibility: Do not contact with strong acids and oxidizers.

  • Environment: WGK 1 (slight hazard to water); no bioaccumulation.

CRITICAL NOTICES:

  1. Chloride-free nature: Calcium formate is a safe alternative to corrosive additives such as calcium chloride. It is therefore preferred in reinforced concrete structures and steel-reinforced precast elements.

  2. Early strength: Particularly in winter concreting, it can reduce setting time by 30-50% at low temperatures (+5°C to -5°C).

  3. Feed additive approval: Approved as a feed additive by the European Union (EFSA), USA (FDA), and Turkey (TKG). Clinically shown to reduce diarrhea incidence in swine feeds.

  4. Water solubility: High water solubility provides homogeneous distribution in concrete mixtures and ease of use in liquid formulations.

  5. Shelf life: Can be stored for 24 months in original packaging under dry conditions. Exposure to moisture may cause caking and loss of flowability.

  6. Dosage information: Used at 0.5-2.0% of cement weight in concrete. Must be optimized through concrete trials prior to use.

Important Disclaimer: This Technical Data Sheet (TDS) is for informational purposes only. The information provided is based on available data and is believed to be accurate. However, the user is solely responsible for determining the suitability of the product for their specific applications and for complying with all applicable regulations and safety requirements. For complete safety, handling, storage, and regulatory compliance information, always refer to the official Safety Data Sheet (SDS/MSDS) provided by the manufacturer/supplier. Users are obligated to test the product in their own processes and applications. All local, national, and international occupational health and safety regulations must be followed when working with calcium formate.

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