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Bupivacaine Hydrochloride, Bupivacaine HCl, Bupivacaine Base, 38396-39-3, 2180-92-9

Bupivacaine Hydrochloride, Bupivacaine HCl, Bupivacaine Base, 38396-39-3, 2180-92-9

BUPIVACAINE HYDROCHLORIDE

PRODUCT IDENTIFIER INFORMATION

Parameter Information
Product Name Bupivacaine Hydrochloride
Chemical Name (IUPAC) (RS)-1-Butyl-N-(2,6-dimethylphenyl)piperidine-2-carboxamide hydrochloride
CAS Number 38396-39-3 (HCl salt) / 2180-92-9 (Base)
EC Number (EINECS) 253-912-7
Molecular Formula (Base) C18H28N2O
Molecular Formula (HCl Salt) C18H29ClN2O
Molecular Weight (Base) 288.43 g/mol
Molecular Weight (HCl Salt) 324.89 g/mol

SECTION 1: CHEMICAL IDENTITY AND DESCRIPTION

Parameter Information
Chemical Name (IUPAC) (RS)-1-Butyl-N-(2,6-dimethylphenyl)piperidine-2-carboxamide hydrochloride
Synonyms Bupivacaine Hydrochloride, Bupivacaine HCl
Trade Names Marcaine, Sensorcaine, Vivacaine, Exparel (liposomal form)
CAS Number (HCl Salt) 38396-39-3
CAS Number (Base) 2180-92-9
EC Number (EINECS) 253-912-7
Molecular Formula (Base) C18H28N2O
Molecular Formula (HCl Salt) C18H29ClN2O
Molecular Weight (Base) 288.43 g/mol
Molecular Weight (HCl Salt) 324.89 g/mol
Chemical Class Amide-type local anesthetic
Chirality Racemic mixture (R-(+)- and S-(-)-enantiomers)
Physical State (20°C) Solid (white crystalline powder)
Odor Odorless
Taste Bitter; temporary numbness on tongue

SECTION 2: PHYSICAL AND CHEMICAL PROPERTIES

Property Value Test Method
Appearance White crystalline powder Visual
Odor Odorless Olfactometric
Taste Bitter; temporary numbness Sensory
Molecular Weight (HCl Salt) 324.89 g/mol Calculated
Molecular Weight (Base) 288.43 g/mol Calculated
Melting Point (HCl Salt) 250 – 260°C DSC
Melting Point (Base) 107 – 108°C DSC
pKa (25°C) ~8.1 Potentiometric
Solubility in Water (HCl Salt) Soluble (~50 g/L) Gravimetric
Solubility in Ethanol Soluble General Method
Solubility in Chloroform Soluble General Method
pH (1% HCl salt solution, 25°C) 4.0 – 6.0 pH Meter
Partition Coefficient (Log P) ~3.41 (base) Calculated
Protein Binding ~95% (primarily α1-acid glycoprotein) -
Stability Stable under normal conditions; light-sensitive  

SECTION 3: CHEMICAL PROPERTIES AND REACTIVITY

Parameter Information
Chemical Character Amide-type local anesthetic; weak base (pKa ~8.1); lipophilic (Log P ~3.41)
Stability Stable under normal conditions; light-sensitive; resistant to autoclave sterilization
Hydrolysis Amide bond much more resistant to hydrolysis compared to ester-type anesthetics
Decomposition Products (Heating) CO, CO2, NOx, HCl
Incompatible Materials Strong oxidizing agents, strong alkalis
Reaction with Alkali Free base precipitates
Hazardous Polymerization Does not occur

SECTION 4: LOCAL ANESTHETICS COMPARISON

Property Bupivacaine Lidocaine Procaine Ropivacaine Levobupivacaine
CAS Number 38396-39-3 137-58-6 59-46-1 98717-15-8 27262-47-1
Class Amide Amide Ester Amide Amide (S-isomer)
Onset of Action Slow (5-10 min) Fast (2-5 min) Moderate (5-10 min) Slow (5-15 min) Slow (5-10 min)
Duration of Action Long (3-8 hrs) Medium (1-2 hrs) Short (30-60 min) Long (3-6 hrs) Long (3-8 hrs)
pKa 8.1 7.9 8.9 8.1 8.1
Maximum Dose 2 mg/kg 4.5 mg/kg 10 mg/kg 3 mg/kg 2 mg/kg
Cardiotoxicity High Low Low Moderate Low (S-isomer)
Sensory/Motor Separation Poor Moderate Poor Good Good
Allergy Risk Very Low Very Low Moderate (PABA) Very Low Very Low
Primary Use Epidural, spinal, peripheral nerve block Infiltration, topical Infiltration (historical) Epidural, spinal Epidural, spinal

SECTION 5: PHARMACOLOGICAL PROPERTIES AND MECHANISM OF ACTION

Property Description
Mechanism of Action Blocks voltage-gated sodium (Na+) channels; prevents action potential generation and conduction in nerve cells
Anesthetic Class Amide-type local anesthetic (amino amide)
Onset of Action Slow (5-10 minutes)
Duration of Action Long (3-8 hours); up to 72 hours in liposomal form
Lipophilic Property Highly lipophilic (Log P ~3.41); more lipophilic than lidocaine
Protein Binding ~95% (primarily α1-acid glycoprotein)
Vasodilator Effect Less vasodilation than lidocaine and procaine
Metabolism Metabolized in liver by CYP3A4 and CYP2C9 enzymes; N-dealkylation
Half-Life 2.7 hours (adults); 8 hours (neonates)
Cardiotoxicity Cardiotoxic at high doses; slow dissociation from sodium channels (fast-in, slow-out)
Sensory/Motor Separation Limited sensory-motor separation at low concentrations

SECTION 6: PRIMARY APPLICATION AREAS

Sector / Application Use Typical Concentration / Dose
Surgery - Epidural Epidural anesthesia (surgical) 0.5 – 0.75%
Surgery - Spinal Spinal anesthesia 0.5% (hyperbaric/isobaric)
Obstetrics - Epidural Epidural analgesia (labor pain) 0.0625 – 0.25%
Peripheral Nerve Block Brachial plexus, femoral, sciatic nerve block 0.25 – 0.5%
Post-operative Analgesia Wound infiltration, nerve block 0.25 – 0.5%
Chronic Pain Management Trigeminal neuralgia, complex regional pain syndrome 0.25 – 0.5%
Liposomal Bupivacaine (Exparel) Post-operative analgesia (up to 72 hours) 133-266 mg
Dentistry Long-duration dental procedures 0.5% (with epinephrine)
Veterinary Local infiltration, nerve block 0.25 – 0.5%

SECTION 7: QUALITY SPECIFICATIONS (PHARMACEUTICAL GRADE - USP/EP)

Parameter Specification Test Method
Appearance White crystalline powder Visual
Odor Odorless Olfactometric
Purity (C18H29ClN2O, Dry Basis) 98.5 – 101.5% HPLC / Titrimetric
Melting Range (HCl Salt) 250 – 260°C DSC / Capillary Tube
Loss on Drying (105°C, 2 hours) ≤ 0.5% Gravimetric
pH (1% solution, 25°C) 4.0 – 6.0 pH Meter
Chloride (Cl-) 10.5 – 11.3% Argentometric
Sulfated Ash ≤ 0.1% Gravimetric
Heavy Metals (as Pb) ≤ 20 ppm ICP-MS / USP <231>
Lead (Pb) ≤ 3 ppm ICP-MS
Arsenic (As) ≤ 3 ppm ICP-MS
Mercury (Hg) ≤ 1 ppm ICP-MS
Cadmium (Cd) ≤ 1 ppm ICP-MS
2,6-Dimethylaniline ≤ 100 ppm HPLC
Related Substances (Total) ≤ 1.0% HPLC
Enantiomeric Purity (for Levobupivacaine) S-isomer ≥ 99% Chiral HPLC
Total Microbial Count ≤ 100 CFU/g USP <61>
Yeast and Mold ≤ 10 CFU/g USP <61>
E. coli Negative in 1g USP <62>
Salmonella spp. Negative in 25g USP <62>

SECTION 8: TOXICOLOGICAL PROFILE

Parameter Value
Acute Oral Toxicity (LD50, Rat) ~200-400 mg/kg
Acute Dermal Toxicity (LD50, Rabbit) > 2,000 mg/kg
Skin Irritation Mild irritant
Eye Irritation Irritant
Respiratory Irritation Inhalation of dust may cause mechanical irritation
Carcinogenicity Not classified (IARC, NTP)
Mutagenicity Negative in in vitro tests
Reproductive Toxicity Fetal effects at high doses; use with caution during pregnancy
Cardiotoxicity Significantly cardiotoxic at high doses; ventricular arrhythmia, cardiac arrest
Neurotoxicity At high doses: dizziness, tinnitus, convulsions, loss of consciousness
Systemic Toxicity More toxic than lidocaine; narrow safety margin

SECTION 9: GHS CLASSIFICATION AND LABELING

GHS Classification (compliant with 1272/2008/EC):

Hazard Class Category H-Statement
Acute Toxicity (Oral) Category 3 H301
Acute Toxicity (Dermal) Category 3 H311
Acute Toxicity (Inhalation) Category 3 H331

Signal Word: DANGER

Hazard Pictograms: GHS06 (Skull and Crossbones)

Hazard Statements (H-Codes):

Code Statement
H301 Toxic if swallowed
H311 Toxic in contact with skin
H331 Toxic if inhaled

Precautionary Statements (P-Codes):

Code Statement
P261 Avoid breathing dust/fume/gas
P280 Wear protective gloves/protective clothing/eye protection
P301+P310 IF SWALLOWED: Immediately call a POISON CENTER/doctor
P302+P352 IF ON SKIN: Wash with plenty of water and soap
P304+P340 IF INHALED: Remove person to fresh air and keep comfortable for breathing
P311 Call a POISON CENTER/doctor

SECTION 10: FIRST AID MEASURES

Exposure Route Action to Take
Inhalation Move to fresh air. Seek medical attention if breathing difficulty persists.
Skin Contact Remove contaminated clothing immediately. Wash with plenty of water and soap for at least 15 minutes. Seek medical attention.
Eye Contact Rinse immediately with plenty of water for at least 15 minutes. Remove contact lenses if present. Seek immediate medical attention.
Ingestion Rinse mouth with water. Do NOT induce vomiting. Seek immediate medical attention and show container or label.

SECTION 11: FIREFIGHTING MEASURES

Parameter Information
Fire Hazard Non-flammable
Hazards During Fire CO, CO2, NOx, HCl
Suitable Extinguishing Media Water mist, CO2, dry chemical powder, foam
Special Protective Equipment Self-contained breathing apparatus (SCBA), full protective clothing

SECTION 12: STORAGE AND SHELF LIFE

Parameter Information
Storage Conditions Room temperature (15-25°C), dry, well-ventilated area; light-protected closed packaging
Container Requirements Tightly closed, light-resistant containers
Keep Away From Light, moisture, strong oxidizing agents, strong alkalis
Shelf Life 36-48 months (unopened original packaging under appropriate storage conditions)
Stability Note Resistant to autoclave sterilization; light-sensitive

SECTION 13: PACKAGING OPTIONS

Packaging Type Quantity Material
Aluminum foil pouch (light-protective) 1 kg Laminated aluminum
Aluminum foil pouch (light-protective) 5 kg Laminated aluminum
Fiber drum with PE liner 25 kg Fiberboard + PE
HDPE drum (light-protected) 25-50 kg HDPE

SECTION 14: TRANSPORTATION INFORMATION

Parameter Information
UN Number UN 2811 (Toxic Solid, Organic, n.o.s.)
Hazard Class 6.1 (Toxic Substances)
Packing Group III
ADR/RID UN 2811, Toxic Solid, 6.1, PG III
IMDG Code UN 2811, Toxic Solid, 6.1, PG III
IATA (Air) UN 2811, Toxic Solid, 6.1, PG III
Marine Pollutant No
Transport Temperature Ambient

SECTION 15: REGULATORY STATUS

Region / Authority Status
USA (USP-NF) Official monograph (USP Bupivacaine Hydrochloride)
European Pharmacopoeia Official monograph (Ph. Eur. Bupivacaine Hydrochloride)
USA (FDA) Prescription drug; liposomal form (Exparel) approved
WHO Essential Medicines List Essential medicine (local anesthetic)
Turkey Licensed pharmaceutical active ingredient; prescription drug
DEA / Controlled Substance Not a controlled substance

SECTION 16: OTHER NAMES AND SYNONYMS

Type Name
Chemical Names (RS)-1-Butyl-N-(2,6-dimethylphenyl)piperidine-2-carboxamide; 1-Butyl-2',6'-pipecoloxylidide
Common Names Bupivacaine, Bupivacaine HCl
Trade Names Marcaine, Sensorcaine, Vivacaine, Exparel (liposomal)
Isomeric Forms Levobupivacaine (S-isomer, CAS 27262-47-1); Ropivacaine (S-isomer analog)
CAS Number (HCl Salt) 38396-39-3
CAS Number (Base) 2180-92-9
EC Number 253-912-7

SECTION 17: SUMMARY TABLE

Parameter Value
Product Bupivacaine Hydrochloride
CAS Number 38396-39-3
Molecular Formula (Base) C18H28N2O
Molecular Weight (HCl Salt) 324.89 g/mol
Appearance White crystalline powder
Melting Point 250 – 260°C
pKa ~8.1
Solubility in Water ~50 g/L
Primary Function Amide-type long-acting local anesthetic
Shelf Life 36-48 months
GHS Signal Word Danger
UN Number UN 2811 (Toxic Solid, 6.1, PG III)

SECTION 18: CRITICAL WARNINGS AND BEST PRACTICES

CRITICAL WARNINGS:

  1. Cardiotoxicity: Bupivacaine is significantly more cardiotoxic than lidocaine and procaine. Absolutely avoid intravascular injection.

  2. Narrow Safety Margin: Maximum dose 2 mg/kg; overdose may cause serious cardiac and neurological toxicity.

  3. Toxic: Toxic if swallowed, in contact with skin, or if inhaled. Use protective equipment.

  4. Epidural/Spinal Administration: Should only be administered by experienced clinicians.

  5. Liposomal Form: Liposomal bupivacaine (Exparel) should not be administered simultaneously with free bupivacaine.

BEST PRACTICE RECOMMENDATIONS:

  1. Aspiration: Always aspirate before injection; avoid intravascular injection.

  2. Dose Calculation: Calculate maximum safe dose (2 mg/kg); adjust dose according to patient weight.

  3. Test Dose: Administer test dose with epinephrine before epidural administration.

  4. Cardiac Monitoring: Monitor ECG and vital signs during high-dose administration.

  5. Levobupivacaine Alternative: S-isomer (levobupivacaine) may be preferred for lower cardiotoxicity risk.

LEGAL DISCLAIMER:

The information provided in this document is presented in good faith based on our current knowledge and experience; however, since all usage conditions are beyond our control, it does not constitute a binding specification or warranty. This Technical Data Sheet is for informational purposes only and does not constitute medical advice. Users are obligated to test the suitability for their own applications. For complete safety, storage, handling, transportation, disposal, and regulatory compliance information, refer to the official Safety Data Sheet (SDS/MSDS) provided by the manufacturer/supplier. This product is not intended to diagnose, treat, cure, or prevent any disease.

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