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Dimethyl Dicarbonate, Dimethyl Pyrocarbonate, DMDC, 4525-33-1

Dimethyl Dicarbonate, Dimethyl Pyrocarbonate, DMDC, 4525-33-1

DIMETHYL DICARBONATE (DMDC) – DİMETİL DİKARBONAT

CAS Number: 4525-33-1
EC Number (EINECS): 224-859-8
Molecular Formula: C₄H₆O₅
Molecular Weight: 134.09 g/mol
E Number: E242

SECTION 1: CHEMICAL IDENTITY AND DEFINITION

Parameter Information
Chemical Name (IUPAC) Dimethyl dicarbonate
Other Names DMDC, Dimethyl pyrocarbonate, Dicarbonic acid dimethyl ester, Pyrocarbonic acid dimethyl ester
Chemical Formula C₄H₆O₅
Molecular Weight 134.09 g/mol
CAS Number 4525-33-1
EC Number (EINECS) 224-859-8
E Number E242 (Preservative)
Chemical Class Dicarbonate ester
Appearance Colorless liquid
Odor Sharp, pungent, characteristic
Physical State (20°C) Liquid

SECTION 2: PHYSICAL PROPERTIES

Property Value
Appearance Colorless liquid
Odor Sharp, pungent, characteristic
Molecular Weight 134.09 g/mol
Melting Point 17 °C
Boiling Point 172 °C (decomposes)
Density (20°C) ~1.25 g/cm³
Refractive Index (nD²⁰) 1.392
Solubility in Water Limited (hydrolyzes in aqueous solutions)
Solubility in Organic Solvents Soluble in ethanol, methanol, acetone, ether
Vapor Pressure (20°C) ~0.3 hPa
Flash Point 80 °C
Autoignition Temperature 480 °C

SECTION 3: CHEMICAL PROPERTIES

Property Information
Chemical Formula C₄H₆O₅
Molecular Weight 134.09 g/mol
Chemical Class Dicarbonate ester
Structure Two methoxycarbonyl groups linked by oxygen
SMILES COC(=O)OC(=O)OC
InChI Key HCAJEUSONHSBGS-UHFFFAOYSA-N
Stability Stable in closed containers; hydrolyzes in contact with moisture
Hydrolysis Products Methanol + Carbon dioxide
Incompatible Materials Strong oxidizing agents, strong acids, strong bases, moisture
Reactivity Reacts with water, alcohols, amines

Chemical Structure:

    O       O
    ||      ||
CH₃-O-C-O-C-O-CH₃

SECTION 4: MECHANISM OF ACTION

Parameter Description
Primary Function Antimicrobial preservative; microbial inhibitor
Mechanism Inactivates enzymes and proteins through carboxymethylation of amine and thiol groups
Target Microorganisms Bacteria, yeast, molds
Mode of Action Inhibits cellular metabolism; prevents microbial growth
Hydrolysis Rapidly hydrolyzes to methanol and carbon dioxide; leaves no residues
Hydrolysis Half-Life (Water) < 30 minutes at 20°C
Hydrolysis Half-Life (Beverage) < 2 hours at 20°C

SECTION 5: TECHNICAL FUNCTIONALITY

Property Description
Primary Function Antimicrobial preservative; microbial stabilizer
Effect on Microorganisms Kills or inhibits bacteria, yeast, and molds
Application Added to beverages prior to bottling
Advantages Does not affect taste, color, or aroma
No Residue Hydrolyzes to harmless compounds (methanol + CO₂)
Shelf Life Extension Extends product shelf life significantly
GMP Application Applied under Good Manufacturing Practice

SECTION 6: FOOD INDUSTRY APPLICATIONS (E242)

Application Description
Non-Alcoholic Beverages Soft drinks, carbonated beverages, ready-to-drink teas
Wine Stabilization of wine; prevents refermentation
Fruit Juices Fruit and vegetable juices; prevents microbial spoilage
Flavored Beverages Flavored water, sports drinks
Alcoholic Beverages Wine, cider, other fermented beverages
Tea and Coffee Drinks Ready-to-drink coffee and tea products

SECTION 7: TYPICAL USAGE LEVELS

Application Typical Dosage Maximum Limit
Non-Alcoholic Beverages 200-250 mg/L 250 mg/L
Wine 200-250 mg/L 250 mg/L
Fruit Juices 200-250 mg/L 250 mg/L
Flavored Beverages 200-250 mg/L 250 mg/L
Maximum Allowed 250 mg/L 250 mg/L

SECTION 8: REGULATORY STATUS

Region / Authority Status
European Union (EFSA) Approved as E242
USA (FDA) Approved as GRAS (21 CFR 172.133)
Turkey Approved (Türk Gıda Kodeksi)
JECFA (FAO/WHO) Approved; ADI: 0-0.05 mg/kg bw/day (expressed as methanol)
Codex Alimentarius Approved (INS 242)
Maximum Usage Level 250 mg/L in beverages

SECTION 9: METABOLISM AND RESIDUE INFORMATION

Parameter Information
Hydrolysis Products Methanol + Carbon dioxide
Hydrolysis Rate Rapid; complete within minutes to hours
Residue No residual active substance remains
Methanol Formation 1 mg DMDC forms approximately 0.24 mg methanol
Methanol Safety Methanol formation is within safe limits at normal usage levels
Excretion Methanol is metabolized and excreted normally

SECTION 10: TOXICOLOGICAL INFORMATION

Parameter Value
Oral LD50 (Rat) 250-500 mg/kg
Dermal LD50 (Rabbit) > 2,000 mg/kg
Inhalation LC50 (Rat) 5.5 mg/L (4 hours)
ADI (Acceptable Daily Intake) 0-0.05 mg/kg bw/day (expressed as methanol)
Carcinogenicity Not classified as carcinogenic
Mutagenicity Negative in standard tests
Reproductive Toxicity No evidence of adverse effects

SECTION 11: GHS CLASSIFICATION

Hazard Class Category
Acute Toxicity (Oral) Category 4 (H302)
Skin Corrosion/Irritation Category 2 (H315)
Eye Damage/Irritation Category 2 (H319)
Specific Target Organ Toxicity (STOT - SE) Category 3 (H335)
Signal Word Warning

SECTION 12: HAZARD STATEMENTS (H-CODES)

Code Statement
H302 Harmful if swallowed
H315 Causes skin irritation
H319 Causes serious eye irritation
H335 May cause respiratory irritation

SECTION 13: PRECAUTIONARY STATEMENTS (P-CODES)

Code Statement
P261 Avoid breathing vapors
P280 Wear protective gloves/eye protection
P301+P312 IF SWALLOWED: Call a POISON CENTER/doctor if you feel unwell
P302+P352 IF ON SKIN: Wash with plenty of soap and water
P305+P351+P338 IF IN EYES: Rinse cautiously with water for several minutes; remove contact lenses if present and easy to do; continue rinsing

SECTION 14: FIRST AID MEASURES

Exposure Route Action
Inhalation Move to fresh air. If respiratory irritation persists, seek medical attention.
Skin Contact Wash with plenty of soap and water. Remove contaminated clothing.
Eye Contact Rinse immediately with plenty of water for at least 15 minutes. Seek medical attention.
Ingestion Rinse mouth. Do not induce vomiting. Seek medical attention.

SECTION 15: STORAGE AND SHELF LIFE

Parameter Information
Storage Conditions Cool (15-25°C), dry, well-ventilated area
Container Requirements Tightly closed, moisture-proof containers
Protect From Moisture, strong oxidizing agents, strong acids, strong bases
Shelf Life 12-24 months (unopened original packaging)
Stability Note Hydrolyzes in contact with moisture; keep tightly sealed

SECTION 16: PACKAGING OPTIONS

Packaging Type Quantity Material
Glass bottle 1 kg Amber glass
Glass bottle 5 kg Amber glass
Plastic drum 25 kg HDPE
Plastic drum 200 kg HDPE
IBC Container 1,000 kg Plastic

SECTION 17: TRANSPORT INFORMATION

Parameter Information
UN Number Not regulated (not dangerous goods)
Hazard Class Not applicable
Packing Group Not applicable
ADR/RID Not regulated
IMDG Code Not regulated
IATA (Air) Not regulated
Marine Pollutant No

SECTION 18: FIRE-FIGHTING MEASURES

Parameter Information
Fire Hazard Combustible liquid
Flash Point 80 °C
Autoignition Temperature 480 °C
Suitable Extinguishing Media CO₂, dry chemical powder, alcohol-resistant foam, water spray
Specific Hazards When heated, emits CO, CO₂, toxic fumes
Protective Equipment Self-contained breathing apparatus (SCBA), full protective clothing

SECTION 19: ACCIDENTAL SPILLAGE AND CLEANUP

Parameter Information
Personal Protection Nitrile gloves, protective goggles, chemical-resistant clothing
Cleaning Methods Absorb with inert material (sand, vermiculite); dispose in sealed containers
Environmental Precautions Prevent entry into drains, soil, and surface waters
Waste Disposal According to local regulations; incineration at licensed facilities

SECTION 20: SUMMARY AND CRITICAL NOTES

Product Summary

Parameter Value
Product Dimethyl Dicarbonate (DMDC)
CAS Number 4525-33-1
E Number E242
Appearance Colorless liquid
Molecular Weight 134.09 g/mol
Primary Function Antimicrobial preservative
Maximum Usage 250 mg/L in beverages
ADI 0-0.05 mg/kg bw/day (as methanol)

Critical Notes

  1. Effective Antimicrobial: DMDC is a powerful antimicrobial agent effective against bacteria, yeast, and molds.

  2. No Residue: Hydrolyzes rapidly to methanol and carbon dioxide; leaves no active residues in the final product.

  3. Taste Neutrality: Does not affect taste, color, or aroma of beverages.

  4. Regulatory Status: Approved in EU (E242), USA (GRAS), JECFA, and Codex Alimentarius.

  5. Maximum Usage: Limited to 250 mg/L in beverages under GMP.

  6. ADI (as Methanol): 0-0.05 mg/kg body weight/day.

  7. Hydrolysis Products: Methanol + CO₂; methanol formed is within safe limits.

  8. Application Timing: Must be added prior to bottling; requires contact time for efficacy.

  9. Handling: Moisture-sensitive; must be stored in tightly sealed containers.

  10. Common Applications: Soft drinks, wine, fruit juices, ready-to-drink teas, sports drinks.

IMPORTANT DECLARATION: This Technical Data Sheet (TDS) is for informational purposes only and has been prepared based on available technical data. The user is responsible for determining the product's suitability for their specific application and for complying with all local, national, and international regulations. For complete safety, storage, use, transport, waste, and regulatory compliance information, refer to the official Safety Data Sheet (SDS/MSDS) provided by the manufacturer/supplier.

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