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Tripropylene Glycol Diacrylate, TPGDA, 42978-66-5

Tripropylene Glycol Diacrylate, TPGDA, 42978-66-5

TRIPROPYLENE GLYCOL DIACRYLATE (TPGDA)

CAS Number: 42978-66-5
EC Number (EINECS): 255-982-0
Molecular Formula: C₁₅H₂₄O₆
Molecular Weight: 298.33 g/mol
Chemical Class: Diacrylate monomer

SECTION 1: PRODUCT IDENTIFICATION AND CHEMICAL IDENTITY

Parameter Description
Chemical Name (IUPAC) 2-Propenoic acid, tripropylene glycol ester
Other Names TPGDA, Tripropylene Glycol Diacrylate, Tripropylene Glycol Diester Acrylic Acid, Acrylic Acid Tripropylene Glycol Ester, Acrylate Monomer TPGDA
CAS Number 42978-66-5
EC Number (EINECS) 255-982-0
Molecular Formula C₁₅H₂₄O₆
Molecular Weight 298.33 g/mol
Chemical Class Diacrylate monomer
Structure CH₂=CHCOO[CH₂CH(CH₃)O]₃COCH=CH₂
Appearance Clear, colorless liquid
Odor Mild acrylate odor
Functionality Two (diacrylate)

SECTION 2: PHYSICAL AND CHEMICAL PROPERTIES

Property Value / Range
Molecular Formula C₁₅H₂₄O₆
Molecular Weight 298.33 g/mol
Appearance Clear, colorless liquid
Odor Mild acrylate odor
Density (25°C) ~1.08 g/cm³
Boiling Point >250°C
Freezing Point -15°C
Flash Point ~110°C (closed cup)
Viscosity (25°C) 25–50 mPa·s (cP)
Purity ≥ 98.0%
Acid Content ≤ 0.02%
Water Content ≤ 0.2%
Color (APHA) ≤ 30
Functionality 2 (diacrylate)
Theoretical Molecular Weight ~300 g/mol
Refractive Index ~1.452
Surface Tension ~30-35 mN/m
Vapor Pressure (20°C) <0.01 mmHg (very low)

SECTION 3: CHEMICAL PROPERTIES AND REACTIONS

Property Description
Chemical Class Diacrylate monomer
Functional Groups Two acrylate groups (C=C), ether linkages
Reactivity High; readily polymerizes under UV/EB
Polymerization Free-radical polymerization (UV, EB, heat, initiator)
Copolymerization Copolymerizes with other acrylates, methacrylates, styrene
Thermal Decomposition > 200°C releases CO, CO₂, and irritant vapors
Hydrolysis Slow hydrolysis in acidic/basic media
Oxidation May form peroxides in air
Polymerization Inhibitor 200–400 ppm MEHQ (hydroquinone monomethyl ether)

4.1. Key Reactions

Reaction Type Description
Radical Polymerization UV/EB or heat → Crosslinked network
Copolymerization With other acrylates, methacrylates, styrene
Hydrolysis Acrylic acid + Tripropylene glycol
Michael Addition Reacts with nucleophiles at β-carbon

4.2. Polymerization Inhibition

Parameter Information
Stabilizer 200–400 ppm MEHQ
Stabilizer Function Prevents premature free-radical polymerization
Storage Temperature 15–25°C
Inhibitor Removal Can be removed by distillation

SECTION 5: MAJOR APPLICATIONS AND END-USES

5.1. UV/EB Curable Coatings (Most Important Application)

Application Function Suitability
UV Curable Coatings Reactive diluent, crosslinker High
EB Curable Coatings Reactive diluent, crosslinker High
Industrial Coatings Reactive diluent High
Wood Coatings Reactive diluent High
Plastic Coatings Reactive diluent High

5.2. UV Curable Adhesives

Application Function Suitability
Laminating Adhesives Reactive diluent High
Pressure-Sensitive Adhesives Reactive diluent High
Structural Adhesives Reactive diluent High

5.3. Printing Inks and Varnishes

Application Function Suitability
UV Curable Printing Inks Reactive diluent High
Varnishes Reactive diluent High
Flexographic Inks Reactive diluent High
Offset Inks Reactive diluent High

5.4. Electronics and Specialty Polymers

Application Function Suitability
Electronic Encapsulation Reactive diluent, crosslinker High
Optical Fiber Coatings Reactive diluent High
3D Printing Resins Reactive diluent High
Photoresists Reactive diluent High

5.5. Composites and Polymer Modification

Application Function Suitability
Composite Materials Reactive diluent High
Polymer Modification Crosslinker High
Flexible Plastics and Films Reactive diluent High

SECTION 6: INDUSTRY SUITABILITY MATRIX

Industry Suitability Explanation
UV Coatings High Reactive diluent, crosslinker
UV Adhesives High Reactive diluent
Printing Inks High Reactive diluent
Electronics High Encapsulation, optical fiber coatings
3D Printing High Reactive diluent
Composites High Reactive diluent
Automotive High UV coatings
Cosmetics Not suitable Not used in cosmetics
Food Not suitable Not used as food additive

SECTION 7: COMPARISON WITH OTHER ACRYLATE MONOMERS

Property TPGDA HDDA TMPTA PETA
Functionality 2 2 3 4
Molecular Weight 298 g/mol 226 g/mol 296 g/mol 352 g/mol
Viscosity (25°C) 25–50 cP 5–10 cP 50–100 cP 100–300 cP
Flexibility High Moderate Low Very low
Hardness Moderate High Very High Excellent
Chemical Resistance Good Good Excellent Excellent
Primary Use Coatings, adhesives Coatings Coatings, inks Coatings, inks

SECTION 8: OTHER NAMES AND IDENTIFIERS

Type Name / Description
IUPAC Name 2-Propenoic acid, tripropylene glycol ester
Commercial Names TPGDA, Tripropylene Glycol Diacrylate
Synonyms Tripropylene glycol diester acrylic acid, Acrylic acid tripropylene glycol ester, Acrylate monomer TPGDA
CAS Number 42978-66-5
EC Number 255-982-0
HS Code 29161200

SECTION 9: TOXICOLOGY AND HEALTH EFFECTS

Parameter Value / Description
GHS Classification Warning
Signal Word Warning
Hazard Statements H315 (Causes skin irritation), H317 (May cause allergic skin reaction), H319 (Causes serious eye irritation), H335 (May cause respiratory irritation)
Precautionary Statements P261 (Avoid breathing dust/fume/gas/mist/vapors/spray), P280 (Wear protective gloves/protective clothing/eye protection/face protection), P302+P352 (IF ON SKIN: Wash with plenty of water), P305+P351+P338 (IF IN EYES: Rinse cautiously with water)
Oral LD50 (Rat) > 2,000 mg/kg
Dermal LD50 (Rabbit) > 2,000 mg/kg
Skin Irritation Irritant
Eye Irritation Irritant
Skin Sensitization Positive (allergic contact dermatitis)
Mutagenicity Negative
Carcinogenicity Not classified
Target Organs Skin, eyes, respiratory system

SECTION 10: SAFETY AND STORAGE

Parameter Information
Storage Conditions Cool, dry, well-ventilated area
Temperature 15–25°C (store under inert atmosphere)
Container Tightly closed, dark, plastic (HDPE) drums, IBC tanks
Special Requirements Must contain inhibitor (MEHQ); avoid extreme temperatures
Sunlight Protection Protect from direct sunlight
Air Exposure Limit air exposure (polymerization risk)
Shelf Life 12 months (under recommended conditions)
Packaging 200 kg drum, 1000 kg IBC, ISO tank

SECTION 11: TRANSPORT INFORMATION

Parameter Information
UN Number Not regulated (not classified as dangerous goods)
Hazard Class Not applicable
Packing Group Not applicable
Proper Shipping Name Tripropylene Glycol Diacrylate
ADR/RID Not regulated
IMDG Code Not regulated
IATA (Air) Not regulated
Marine Pollutant No

SECTION 12: FIRE-FIGHTING MEASURES

Parameter Information
Fire Hazard Combustible liquid (flash point ~110°C)
Extinguishing Media Water fog, foam, CO₂, dry chemical
Special Hazards When heated, releases CO, CO₂, and irritant vapors
Decomposition Products CO, CO₂, acrylate vapors
Protective Equipment Self-contained breathing apparatus (SCBA), full protective clothing
Explosion Risk Vapor/air mixtures may be explosive at high temperatures

SECTION 13: ACCIDENTAL RELEASE AND CLEANUP

Parameter Information
Personal Protection Gloves, safety goggles, face shield, protective clothing
Ventilation Increase ventilation; evacuate area
Cleanup Methods Absorb with inert absorbent material; collect in sealed containers
Environmental Precautions Prevent entry into drains and water bodies
Waste Disposal According to local regulations; incineration (hazardous waste)

SECTION 14: FIRST AID MEASURES

Exposure Route Action
Inhalation Move to fresh air. Administer oxygen if breathing difficulty. Seek medical attention.
Skin Contact Remove contaminated clothing. Wash with soap and plenty of water for at least 15 minutes. Seek medical attention.
Eye Contact Rinse with plenty of water for at least 15 minutes. Seek medical attention.
Ingestion Do NOT induce vomiting. Drink plenty of water. Seek medical attention.

SECTION 15: REGULATORY INFORMATION

Region / Authority Status
EU REACH Registered
Turkey KKDİK Registration required
USA TSCA Listed
EINECS 255-982-0
WGK (Germany) 1 (slight hazard to water)
RoHS Compliant
California Prop 65 Not listed

SECTION 16: SUMMARY AND CRITICAL WARNINGS

Product Summary

Parameter Value
Product Tripropylene Glycol Diacrylate (TPGDA)
CAS 42978-66-5
Appearance Clear, colorless liquid
Density ~1.08 g/cm³
Viscosity (25°C) 25–50 cP
Functionality 2 (diacrylate)
Key Industries UV coatings, adhesives, inks, electronics

CRITICAL WARNINGS

  1. UV/EB Curable Monomer: TPGDA is a widely used difunctional reactive diluent in UV and electron beam (EB) curable systems.

  2. Balanced Properties: Provides high reactivity, flexibility, and excellent adhesion. Offers a good balance between hardness and flexibility.

  3. Low Viscosity: Low viscosity (25–50 cP) facilitates its use as a reactive diluent in formulations.

  4. Polymerization Risk: Readily polymerizes; always contains inhibitor (MEHQ). Keep away from heat and light.

  5. Skin Sensitizer: TPGDA may cause allergic skin reactions (H317). Appropriate PPE required.

  6. Low Volatility: Low vapor pressure and high boiling point (>250°C) provide low volatility.

  7. Storage: Store in cool, dark, well-ventilated areas. Shelf life is 12 months.

  8. Hydrolysis: Slow hydrolysis in acidic/basic media. Protect from moisture.

  9. Alternatives: HDDA provides lower viscosity, TMPTA provides higher functionality and hardness. Selection depends on application.

  10. Regulatory Status: Not classified as dangerous goods for transport. Avoid release to the environment.

IMPORTANT DISCLAIMER: This Technical Data Sheet (TDS) is for informational purposes only and is based on available technical data. The user is solely responsible for determining the product's suitability for their specific application and for complying with all applicable local, national, and international regulations. TPGDA readily polymerizes and is a known skin sensitizer! For complete safety, storage, handling, transportation, disposal, and regulatory compliance information, always refer to the official Safety Data Sheet (SDS/MSDS) provided by the manufacturer/supplier. Users are responsible for testing the product in their own processes and applications. All local, national, and international regulations must be followed when working with TPGDA.

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