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Polyvinyl Acetate, Vinyl Acetate Homopolymer, Vinyl Acetate Resin, White Glue, Wood Glue, PVAc, 9003-20-7

Polyvinyl Acetate, Vinyl Acetate Homopolymer, Vinyl Acetate Resin, White Glue, Wood Glue, PVAc, 9003-20-7

TECHNICAL DATA SHEET (TDS)

Polyvinyl Acetate (PVAc)

CAS Number: 9003-20-7
Chemical Formula: (C₄H₆O₂)ₙ
Repeat Unit: -CH₂CH(O₂CCH₃)-
Synonyms: PVAc, PVA, Vinyl Acetate Homopolymer, Vinyl Acetate Resin, White Glue, Wood Glue

1. CHEMICAL IDENTITY

Parameter Information
Product Name Polyvinyl Acetate
CAS Number 9003-20-7
Chemical Formula (C₄H₆O₂)ₙ
Repeat Unit -CH₂CH(O₂CCH₃)-
Polymer Type Thermoplastic, Atactic, Amorphous
Synonyms PVAc, PVA, Vinyl Acetate Homopolymer, Vinyl Acetate Resin, White Glue, Wood Glue

2. PHYSICAL PROPERTIES

Parameter Value
Physical State (20°C) Liquid (emulsion) or Solid (granules/beads)
Color White (emulsion) to colorless/pale yellow (solid)
Appearance Milky white emulsion or transparent granules
Odor Slight characteristic (emulsion); odorless (solid)
Density (25°C) 1.18 – 1.19 g/cm³
Glass Transition Temperature (Tg) 28 – 45°C (typically ~30-32°C)
Softening Point 30 – 50°C (depends on molecular weight)
Refractive Index (20°C) 1.462 – 1.467
Minimum Film Forming Temperature (MFT) ~18°C (unplasticized)

3. SOLUBILITY PROPERTIES

Solvent Solubility
Water Insoluble (emulsion/dispersion form only)
Acetone Soluble
Chloroform Soluble
Toluene Soluble
Tetrahydrofuran (THF) Soluble
Low Molecular Weight Alcohols Soluble
Esters Soluble
Aliphatic Hydrocarbons Insoluble
Mineral Oils Insoluble

4. THERMAL AND MECHANICAL PROPERTIES

Parameter Value
Glass Transition Temperature (Tg) 28 – 45°C
Minimum Film Forming Temperature (MFT) ~18°C (unplasticized)
Softening Point 40 – 50°C
Decomposition Temperature >150°C
Molecular Weight (Mw) 80,000 – 500,000 (grade dependent)

5. CHEMICAL PROPERTIES AND REACTIVITY

Parameter Description
pH (emulsion) 3.0 – 5.5 (slightly acidic)
Hydrolytic Sensitivity Sensitive to hydrolysis by bases (releases acetic acid)
Hydrolysis Reaction Over time or with base: PVAc → Polyvinyl Alcohol (PVOH) + Acetic Acid
Saponification Value 260 – 270
UV Resistance Good (resistant to yellowing)
Biodegradability Potentially biodegradable (ongoing research)

6. PRODUCTION PROCESS

Step Description
Raw Material Vinyl Acetate Monomer (VAM – CAS 108-05-4)
VAM Production Ethylene + Acetic acid + Oxygen → Palladium-catalyzed oxidative addition → VAM
Emulsion Polymerization VAM + Water + Surfactant + Initiator → Free radical polymerization → PVAc emulsion
Suspension Polymerization VAM + Water + Suspending agent (e.g., partially hydrolyzed PVA) → Solid PVAc granules
Purification Vacuum drying, steam stripping, washing (removes residual monomer and catalyst)

7. TYPICAL PRODUCT SPECIFICATIONS

Parameter Emulsion Grade Solid Grade
Solids Content 50 – 55% >99%
Viscosity 500 – 20,000 cP
pH 3.0 – 5.5
Particle Size 0.2 – 2.0 μm 100 – 500 μm
Molecular Weight (Mw) 80,000 – 200,000 100,000 – 500,000

8. FUNCTIONAL PROPERTIES

Function Description
Film Former Forms a flexible, adhesive film after water evaporation
Adhesive High adhesion to porous surfaces (wood, paper, fabric)
Binder Holds pigments and fillers together (paints, coatings)
Flexibility Film flexibility adjustable by adding plasticizers
Water Resistance Forms a water-resistant film after curing
pH Independence Film properties not affected by pH (no ionizable groups)

9. APPLICATIONS – ADHESIVES

Product Type Description
White Glue (Elmer's Glue) Most common household adhesive; for paper, cardboard, wood, leather
Wood Glue Furniture manufacturing, joinery, parquet flooring
Bookbinding Flexible and acid-free; suitable for bookbinding
Packaging Adhesives Carton sealing tapes, label adhesives, box gluing
Carpentry Wood joining, laminated wood production
Hot Melt Adhesives Formulated as EVA copolymers

10. APPLICATIONS – PAINTS AND COATINGS

Application Function
Water-Based Paints (Latex Paints) Film-forming binder resin; binds pigments, provides flexible film
Wall Paints Binder for interior and exterior wall paints
Paper Coatings Coatings for glossy paper, cardboard, packaging paper
Textile Coatings Fabric finishes, linings
Furniture Coatings Wood varnishes and primers

11. APPLICATIONS – PAPER AND PACKAGING

Application Function
Paper Adhesive Envelope, carton, box gluing
Lamination Paper/paper, paper/foil lamination
Frozen Food Packaging Low-temperature flexibility required for frozen food packaging
Cling Film Coatings Barrier properties

12. APPLICATIONS – FOOD INDUSTRY

Application Function Regulatory Status
Chewing Gum Base Polymer matrix providing chewability FDA 21 CFR 172.615 (USA)
Fruit and Vegetable Coating Edible coating preserving freshness Approved in USA, South Korea, Japan
Cheese Coating Mold and moisture barrier Listed as food additive in Germany
Food Additive Technological purpose additive Permitted in Germany

13. APPLICATIONS – PHARMACEUTICAL INDUSTRY

Application Function Commercial Example
Controlled Release Coatings pH-independent coating for extended release Kollicoat® SR 30 D
Matrix Tablets Used as drug release matrix Kollicoat® SR-based formulations
Enteric Coatings PVAc phthalate (PVAP) form protects stomach PVAP enteric coatings
Orally Disintegrating Tablets Bitter taste masking Ibuprofen-containing formulations
Film Coatings Flexible, pH-independent film coatings Kollicoat® SR 30 D

Pharmaceutical Monographs: PVAc has monographs in Ph. Eur. (Poly(Vinyl Acetate) Dispersion 30 Per Cent), USP (Polyvinyl acetate dispersion), and JPE.

14. APPLICATIONS – TEXTILE INDUSTRY

Application Function
Fabric Finishing Provides stiffness and body
Filter Media (Automotive) Binder and stiffener for air intake filters
Nonwoven Fabrics Binder (for applications requiring stiffness)
Woven Fabric Coating Water repellency and durability

15. OTHER APPLICATIONS

Industry Application
Cosmetics Hair sprays, gels (as copolymer with PVP)
Construction Mortar additives, plaster additives
Cigarette Production Cigarette paper adhesive
Wood Composites Binder for particle board, MDF, plywood
Nanofibers for Sensors Gas sensors, emission sensors
Decoupage and Crafts Surface protective coating

16. COMPARISON: PVAc EMULSION vs. PVAc SOLID

Property PVAc Emulsion (Liquid) PVAc Solid (Granules/Beads)
Appearance Milky white liquid White/Transparent granules
Solids Content 50-55% >99%
Usage Form Direct application Melt or dissolve in solvent
Primary Application Adhesives, paints Pharmaceutical coatings, research
Storage +5°C – +30°C Room temperature
Shelf Life 6-12 months 24-36 months

17. ADVANTAGES AND BENEFITS

Advantage Description
Strong Adhesion Excellent adhesion to porous surfaces (wood, paper, fabric)
Flexible Film Adjustable flexibility with plasticizers; not brittle
Water-Based Compatibility Emulsion form directly adds to water-based formulations
Light Stability Resistant to yellowing upon UV exposure
Low Toxicity Safe for food and pharmaceutical applications
Cost-Effective Low-cost polymer; mass production
pH-Independent Performance Film properties not affected by pH
Low Temperature Flexibility With plasticizers, suitable for frozen food packaging

18. LIMITATIONS AND PRECAUTIONS

Limitation Description Precaution
Water Insolubility Only available as emulsion/dispersion
Low Heat Resistance Softens above ~45°C, loses strength Avoid high-temperature applications
Creep (Cold Flow) Deforms under continuous load Do not use for structural load-bearing applications
Poor Moisture Resistance Adhesion strength decreases at high humidity Use indoors or low-humidity applications
Microbial Degradation Microorganisms can degrade PVAc Add preservative; store dry
Acid/Base Hydrolysis Hydrolyzes with bases, releases acetic acid Avoid high pH
Plasticizer Stability Plasticizer migration may reduce flexibility over time Select appropriate plasticizer

19. STORAGE AND HANDLING

Parameter Emulsion Form Solid Form
Storage Temperature +5°C – +30°C 15-25°C (room temperature)
Freeze Protection Do NOT freeze (coagulation) Not required
Heat Protection Do not store above 35°C Do not store above 50°C (caking)
Container Sealed plastic or metal container Original sealed bag/box
Shelf Life 6-12 months 24-36 months
Special Precautions Microbial protection (preservative may be needed) Store in dry environment

20. SUMMARY AND CRITICAL INFORMATION

Description: Polyvinyl Acetate (PVAc, CAS 9003-20-7) is a thermoplastic, atactic polymer produced by free radical polymerization of vinyl acetate monomer. It is available as a white emulsion (liquid) or transparent granules (solid). Density is ~1.19 g/cm³ and glass transition temperature (Tg) is 30-45°C. PVAc offers high adhesion to porous surfaces, flexible film formation, and excellent light stability.

Key Advantages:

  • Strong adhesion – ideal for wood, paper, fabric, leather adhesives

  • Flexible film – flexibility adjustable with plasticizers

  • Full compatibility with water-based systems

  • Low toxicity – safe for food and pharmaceutical applications

  • Resistant to yellowing

  • Low cost

Key Limitations/Precautions:

  • Water insoluble (only emulsion/dispersion form)

  • Low heat resistance (softens above ~45°C)

  • Creep (cold flow) – deformation under continuous load

  • Hydrolysis with bases – may release acetic acid

  • Microbial degradation – may require preservative

Major Applications by Sector:

Sector Applications
Adhesives White glue, wood glue, bookbinding, packaging adhesives
Paints and Coatings Binder in water-based paints, wall paints, paper coatings
Pharmaceutical Controlled release coatings (Kollicoat® SR 30 D), enteric coatings (PVAP)
Food Chewing gum base, fruit/vegetable coatings
Packaging Lamination, frozen food packaging
Textile Fabric finishing, filter media

Pharmaceutical Significance:

PVAc, particularly under the trade name Kollicoat® SR 30 D, is widely used in extended-release pharmaceutical coatings. It has monographs in Ph. Eur., USP, and JPE. The PVAc phthalate (PVAP) form is used in enteric coatings.

Storage:

Form Temperature Special Warning
Emulsion +5°C – +30°C Do NOT freeze
Solid 15-25°C Protect from moisture

Conclusion: Polyvinyl Acetate, discovered in 1912, is a versatile thermoplastic polymer used in a wide range of applications from adhesives and paints to pharmaceutical coatings and food products. Its compatibility with water-based systems, low toxicity, and cost-effectiveness make it an indispensable component of the adhesive and coating industries. In the pharmaceutical field, particularly as Kollicoat® SR 30 D, it is an important excipient for controlled-release coatings, offering pH-independent and flexible film properties.

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