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Triethylene Glycol, Triethyleneglycol, Triglycol, TEG, ​​​​​​​112-27-6

Triethylene Glycol, Triethyleneglycol, Triglycol, TEG, 112-27-6

TECHNICAL DATA SHEET (TDS)

Product Name: Triethylene Glycol (TEG)
Chemical Formula: C₆H₁₄O₄ / HO–CH₂–CH₂–O–CH₂–CH₂–O–CH₂–CH₂–OH
CAS Number: 112-27-6
EINECS Number: 203-953-2
Molecular Weight: 150.17 g/mol

1. PHYSICAL AND CHEMICAL PROPERTIES

Property Value / Range
Appearance (20°C) Colorless, clear, viscous liquid
Odor Mild characteristic, nearly odorless
Freezing Point -4.3 °C to -7.2 °C (pure)
Boiling Point (1013 hPa) 285 – 288 °C
Flash Point (closed cup) 166 °C (PMCC) – 177 °C (Cleveland)
Density (20°C) 1.124 – 1.126 g/cm³
Viscosity (20°C) ~47 mPa·s (cP)
Viscosity (25°C) ~36 mPa·s
Vapor Pressure (20°C) <0.01 hPa
pH (50% in water) 5.5 – 7.5 (neutral)
Solubility Fully miscible with water, alcohols, glycols, ketones; immiscible with hydrocarbons
Log P (octanol/water) -1.75 (hydrophilic)
Autoignition Temperature 371 °C
Thermal Decomposition Slow oxidation above 220°C; acidic products form above 250°C

2. TYPICAL ANALYSIS (Commercial Grade)

Test Typical Value Method
Purity (wt%) ≥99.0 – 99.8 GC
Water Content (Karl Fischer) ≤0.1 % ASTM E203
Color (APHA/Pt-Co) ≤20 ASTM D1209
Acidity (as acetic acid) ≤0.01 % ASTM D1613
Monoethylene + Diethylene Glycol ≤0.5 % GC
Iron Content ≤1 ppm ICP
Ash Content ≤0.01 % ASTM D482

3. THERMODYNAMIC & TRANSPORT PROPERTIES

  • Specific Heat Capacity (20°C): ~2.2 kJ/(kg·K)

  • Heat of Vaporization (at bp): ~450 kJ/kg

  • Thermal Conductivity (20°C): ~0.21 W/(m·K)

  • Dielectric Constant (20°C, 1 kHz): ~23

4. REACTIVITY & COMPATIBILITY

  • Incompatibilities: Strong oxidizers (HNO₃, H₂O₂), concentrated acids (H₂SO₄) – violent exothermic reaction.

  • Corrosion: Compatible with stainless steel (304, 316), carbon steel, aluminum, PP, PE. Long-term contact with copper and brass not recommended (yellow discoloration).

  • Hygroscopicity: Absorbs moisture from air; store in tightly closed containers.

5. MAIN APPLICATIONS

  1. Natural Gas Dehydration: Most common use – absorbs water vapor from natural gas.

  2. Hydraulic Brake Fluids: Provides low volatility and high boiling point.

  3. Plasticizer: For cellulosic films, printing inks, polyurethane elastomers.

  4. Paints & Coatings: Coalescing solvent.

  5. Heat Transfer Fluid: Closed-loop systems.

  6. Gas Processing: Dehydration and aromatic extraction aid.

6. STORAGE & HANDLING

  • Storage Temperature: 15 – 40°C (protect from freezing; crystallization begins below -5°C – warm and mix to re-liquefy)

  • Container Material: Stainless steel, carbon steel, HDPE drum/tank. Use dry air or nitrogen blanket to prevent moisture ingress.

  • Shelf Life: 24 months in original sealed container, below 25°C, away from direct sunlight (monitor color and acidity).

  • Transport Classification: Not classified as dangerous goods (non-flammable, non-toxic).

7. SAFETY SUMMARY

Parameter Value
LD50 oral (rat) ~15 – 17 g/kg (low toxicity)
Skin irritation Mild irritant; prolonged exposure may cause dryness
Eye irritation Mild to moderate irritant
Exposure limit (TWA) 10 mg/m³ (for aerosol/mist)
Biodegradability Readily biodegradable (OECD 301)
Water hazard class (WGK, Germany) 1 (low hazard to water)

Personal Protective Equipment (PPE):

  • Chemical goggles, nitrile gloves, protective clothing.

  • Normal ventilation is sufficient if no splashing risk.

8. REGULATORY STATUS (Example – US/EU)

  • TSCA (USA): Listed

  • EINECS (EU): 203-953-2 (existing substance)

  • AICS (Australia): Listed

  • GHS Classification (EU 1272/2008):

    • Not classified as hazardous (no hazard pictogram required). Some countries may require H316 (mild skin irritation) and H320 (eye irritation) labels.

9. TYPICAL PACKAGING

  • 200 – 250 kg steel drum

  • 1100 – 1250 kg IBC (pallet tank)

  • Bulk: Tanker / isotank (20 – 23 tons)

1. SECTORAL SUITABILITY (Which Industries & Standards)

Sector Suitability / Standards Explanation
Natural Gas GPSA, ISO 18453, NACE Gold standard for dehydration. TEG absorbs water from gas due to low vapor pressure.
Automotive (Brake Fluids) FMVSS 116 (DOT 3, DOT 4), ISO 4925 TEG is reacted with boric acid to form borate esters for high-boiling brake fluids.
Pharmaceutical USP/NF (Triethylene Glycol monograph), Ph. Eur. Excipient (plasticizer, humectant, solvent). For oral, topical, injectable formulations.
Cosmetics & Personal Care EC 1223/2009 (EU Cosmetics Regulation), CIR approved Humectant, solvent, viscosity regulator. Shampoos, lotions, deodorants, creams.
Paints & Coatings REACH, EPA TSCA Coalescing solvent in water-based paints – improves film formation.
Printing Inks EC 1935/2004 (if not food contact) Improves flexibility and regulates drying time.
Heat Transfer Systems ASTM E1177 (coolants) Closed-loop heat transfer fluid, antifreeze additive.
Plastics & Polyurethane RoHS compliant Plasticizer for polyurethane elastomers – provides flexibility.
Textiles OEKO-TEX (limited concentration) Softener, antistatic agent, moisture retainer.
Aerospace MIL-PRF-46170 (hydraulic fluids) Low-temperature fluidity and high-temperature stability.

Food Contact:
TEG is covered under FDA 21 CFR 178.3740 (indirect food contact – extractables in plastics) but is not generally approved as a direct food additive (unlike propylene glycol). Limited use as heat transfer fluid in food processing equipment.

2. USAGE RECIPES (Formulations)

A. Natural Gas Dehydration (Industrial Process)

Parameter Value
TEG Circulation Rate 15 – 30 L TEG / kg water removed
Contactor Temperature 25 – 40 °C (absorption)
Regeneration Temperature 180 – 204 °C (atmospheric)
Vacuum Regeneration 150 – 160 °C (under vacuum)
Regenerated TEG Purity 98.5 – 99.9 %
Dew Point Depression Down to -40 °C

Note: Prevent oxygen ingress (oxidation → acid formation). Maintain pH 6-8.

B. Brake Fluid (DOT 3 / DOT 4) – TEG Borate Ester

Component % by Weight
TEG 50 – 70
Boric Acid (H₃BO₃) 15 – 25
Diethylene Glycol (DEG) 5 – 15
Antioxidant (BHT, etc.) 0.1 – 0.5
Corrosion Inhibitor 0.2 – 1.0

Process:
TEG + Boric acid → esterification at 120-150°C (remove water) → cool → add other components.
Target: Dry boiling point >260°C (DOT 4 requires >230°C).

C. Water-Based Paint (Coalescing Solvent)

Component % by Weight
Acrylic emulsion (50% solids) 70 – 80
TEG 2 – 5
Water 10 – 20
Surfactant 0.5 – 1
Defoamer 0.2 – 0.5

Effect: Lowers minimum film formation temperature (MFFT). TEG acts as a temporary plasticizer after water evaporates.

D. Cosmetic Lotion (Humectant / Solvent)

Component % by Weight
Water 70 – 85
TEG 2 – 5
Glycerin 2 – 5
Emulsifier (polysorbate, etc.) 1 – 3
Preservative (phenoxyethanol) 0.5 – 1
Fragrance 0.1 – 0.3

Note: For cosmetics, use pharmaceutical / cosmetic grade TEG (heavy metals <10 ppm, DEG <0.1%).

E. Heat Transfer Fluid (Closed Loop)

Component % by Volume
TEG 30 – 50
Water 50 – 70
Corrosion inhibitor (nitrite, molybdate) 0.5 – 2
pH adjuster (borax) pH 8.5 – 10.5

Operating Range: -10°C (freeze protection) to +150°C (pressurized system).
TEG alone has lower heat transfer coefficient than water; water mixture is preferred.

3. ALTERNATIVE NAMES (Synonyms)

  • Triethylene Glycol (IUPAC) – TEG (most common abbreviation)

  • 2,2'-(Ethylenedioxy)diethanol

  • Ethylene glycol bis(2-hydroxyethyl ether)

  • Triglycol

  • Triethyleneglycol (combined spelling)

  • Glycol bis(hydroxyethyl ether)

  • 3,6-Dioxaoctane-1,8-diol (systematic)

  • CAS names: 1,2-Bis(2-hydroxyethoxy)ethane; 2,2'-Ethylenedioxydiethanol

Trade Names (Examples):

  • Carbowax™ (Dow) – Low molecular weight PEG fraction

  • Glycol TEG (Huntsman)

  • Triethylene Glycol (Shell Chemical)

  • TEG (SABIC)

  • Triethylene Glycol (INEOS)

  • Pluracol® E series (BASF) – Some are PEG blends

4. ALTERNATIVE PRODUCTS (Substitutes for TEG)

Application Alternative Advantage / Disadvantage
Natural Gas Dehydration DEG (Diethylene Glycol) Lower viscosity, lower boiling point, higher vapor loss. TEG has better thermal stability.
  MEG (Monoethylene Glycol) Low cost but very volatile, high losses. Preferred for hydrate inhibition in cold climates.
  Ionic Liquids (e.g., [EMIM][Tf₂N]) Very low vapor pressure, high selectivity, but very expensive, not yet widespread.
Brake Fluid DEG + Borate Ester Lower viscosity, lower boiling point. TEG gives higher performance (DOT 4).
  PEG (Polyethylene Glycol 200-400) Higher viscosity, better lubrication. More expensive than TEG.
Plasticizer (Aqueous systems) Propylene Glycol (PG) Lower toxicity, food contact approved, but higher cost.
  Dipropylene Glycol (DPG) Lower hygroscopicity, preferred in some coatings.
  Texanol™ (2,2,4-Trimethyl-1,3-pentanediol monoisobutyrate) Very effective coalescent, lower water solubility, but VOC restrictions apply.
Heat Transfer Fluid Propylene Glycol (PG) Less toxic, preferred in food processing. More expensive than TEG, similar low-temperature performance.
  Ethylene Glycol (EG) Lowest cost, best heat transfer, but high toxicity.
Cosmetics / Pharma Propylene Glycol (PG) Lower skin irritation potential, more widely accepted.
  Glycerin (Glycerol) Natural origin, higher viscosity, sweeter taste.
  Butylene Glycol Lighter feel, more expensive.
Paint / Ink DPG (Dipropylene Glycol) Less hygroscopic, better water resistance.
  PG Lower toxicity, but higher volatility.

5. RECOMMENDATIONS (Important Warnings & Practical Advice)

Storage & Handling

  • Protect from Moisture: TEG is highly hygroscopic. Store under dry air or nitrogen blanket. Open TEG absorbs 1-2% water quickly.

  • Freeze Protection: Freezes around -7°C. Crystallization can expand and damage tanks. Use heated storage (15-40°C) or heat tracing.

  • Material Compatibility: HDPE, stainless steel (304/316), carbon steel are suitable. EPDM gaskets may swell – use Viton® or PTFE seals.

Process & Quality Control

  • Temperature Limit: Above 220°C in air, TEG slowly oxidizes → acid formation (pH drops, corrosion increases). Use inert gas (N₂) blanket in regeneration units.

  • pH Monitoring: Maintain pH 6-8 in TEG circuits. If pH <5, neutralize (with monoethanolamine) or replace TEG.

  • Contamination Control: In gas applications, H₂S, CO₂, and hydrocarbons accumulate in TEG. Use filtration (activated carbon) and periodic purge.

Health & Safety

  • Skin Contact: Prolonged contact causes dryness and cracking. Use nitrile gloves. Wash with soap and water.

  • Eye Contact: Mild irritant. Rinse eyes with water for 15 minutes.

  • Inhalation: Vapor pressure is very low at room temperature – no risk. Above 180°C, aerosol may form – local exhaust ventilation required.

  • Ingestion: Low toxicity, but large amounts may cause diarrhea and dehydration. Do not induce vomiting; drink water; consult a doctor.

Regulatory & Sustainability

  • Waste Management: TEG is biodegradable, but concentrated TEG should not be drained to sewer. Incineration (with energy recovery) or controlled discharge to wastewater treatment (EWC code: 07 02 99).

  • Substitution for Toxicity Concerns: For sensitive applications (food, baby products, pharmaceuticals), use Propylene Glycol or Glycerin. TEG has no reproductive toxicity or carcinogenicity data (Group 4 – probably not carcinogenic, IARC).

  • Cost Optimization: TEG is ~20-30% more expensive than DEG, and 50-80% more expensive than MEG. However, low vapor loss and high thermal stability in gas dehydration make it economical long-term.

Purchasing Advice

  • Purity Grade:

    • Industrial grade (99%) → Natural gas, heat transfer, brake fluid

    • Pharmaceutical / Cosmetic grade (99.5%+, DEG <0.1%, EG <0.05%) → Drugs, cosmetics

  • Global Suppliers: Dow, Shell, Huntsman, SABIC, INEOS, BASF, Lotte Chemical

  • Request Certificates: Certificate of Analysis (CoA), DEG/EG content (GC), water content (KF), color (APHA)

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